三甲基-(1-苯乙烯基)硅烷合成路线 （共 49 条）
反应条件
pyrolysis under vacuum;
参考文献
Creary, Xavier; Wang, You-Xiong
Tetrahedron Letters, 1989 , vol. 30, # 19 p. 2493 - 2496
反应条件
(i) nBuLi, (ii) /BRN= 1209232/; Multistep reaction;
参考文献
Chan,T.H. et al.
Synthesis, 1976 , p. 801 - 803
反应条件
Yield given. Multistep reaction;
参考文献
Ennis, David S.; Gilchrist, Thomas L.
Tetrahedron, 1990 , vol. 46, # 7 p. 2623 - 2632
反应条件
in tetrahydrofuran
T=30°C; Rate constant;
参考文献
Jones, Steven L.; Stirling, Charles J. M.
Journal of the Chemical Society, Chemical Communications, 1988 , # 17 p. 1153 - 1154
反应条件
in tetrahydrofuran
T=30°C; also in DMF and with α-deuterated compound; Rate constant;
参考文献
Jones, Steven L.; Stirling, Charles J. M.
Journal of the Chemical Society, Chemical Communications, 1988 , # 17 p. 1153 - 1154
反应条件
palladium diacetate; triethylamine; triphenylphosphine
T=110°C; 72 h; var. subst. aryl iodides; Product distribution;
参考文献
Nilsson, Kristina; Hallberg, Anders
Acta Chemica Scandinavica, 1990 , vol. 44, # 3 p. 288 - 290
反应条件
1: 30 percent / CH2Cl2
2: 91 percent / caesium fluoride / dimethylformamide / 5 h / Ambient temperature
View Scheme
参考文献
Atkinson, Robert S.; Kelly, Brian J.
Tetrahedron Letters, 1989 , vol. 30, # 20 p. 2703 - 2704
反应条件
1: 86 percent / AIBN / 1 h / 90 °C
2: 65 percent / (NH4)6Mo7O24*7H2O, 30percent H2O2 / methanol / 16 h / 20 °C
View Scheme
参考文献
Menichetti, Stefano; Stirling, Charles J. M.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 13 p. 1511 - 1515
反应条件
T=34.9°C; ΔG0; Thermodynamic data;
参考文献
Mishima, Masaaki; Ariga, Toshifumi; Tsuno, Yuho; Ikenaga, Kazutoshi; Kikukawa, Kiyoshi
Chemistry Letters, 1992 , # 3 p. 489 - 492
