1: 4-nitro-pyridine N-oxide With dimethyl sulfate in water T=-8 - 70°C; 2 h; Inert atmosphere; 2: potassium cyanide in water 12 h; Inert atmosphere;
参考文献
Hayashi, Masashi; Shiomi, Noriyuki; Funahashi, Yasuhiro; Nakamura, Shuichi
Journal of the American Chemical Society, 2012 , vol. 134, # 47 p. 19366 - 19369
Desjardins, Sylvie Y.; Cavell, Kingsley J.; Hoare, Jason L.; Skelton, Brian W.; Sobolev, Alexander N.; White, Allan H.; Keim, Wilhelm
Journal of Organometallic Chemistry, 1997 , vol. 544, # 2 p. 163 - 174
1: 1.) 90percent H2SO4, 2.) NaNO2 / 1.) 120 deg C, 2 h, 2.) water, 20-25 deg C, 1 h, then 80 deg C, 1 h 2: 90 percent / Na / 2 h / Heating View Scheme
参考文献
Hayashi, Masashi; Shiomi, Noriyuki; Funahashi, Yasuhiro; Nakamura, Shuichi
Journal of the American Chemical Society, 2012 , vol. 134, # 47 p. 19366 - 19369
1: With sulfuric acid T=120°C; 2 h; Inert atmosphere; 2: With sodium nitrite in water T=80°C; 2 h; Inert atmosphere;
参考文献
Hayashi, Masashi; Shiomi, Noriyuki; Funahashi, Yasuhiro; Nakamura, Shuichi
Journal of the American Chemical Society, 2012 , vol. 134, # 47 p. 19366 - 19369
