三乙二醇二(对甲苯磺酸酯)合成路线 （共 90 条）
反应条件
triethylamine in tetrahydrofuran 24 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 11 p. 2082 - 2087
反应条件
potassium iodide; silver(l) oxide in dichloromethane T=0°C; 0.166667 h;
参考文献
Organic Letters, , vol. 4, # 14 p. 2329 - 2332
反应条件
p-toluenesulfonyl chloride; sodium hydroxide in 1,4-dioxane; water
参考文献
Synlett, , # 10 p. 1544 - 1548
反应条件
sodium t-butanolate 10 h; Heating1.) t-BuOH, 80 deg C, 1 h 2.) dioxan, reflux, 10 h;
参考文献
Luk'yanenko, N. G.; Mel'nik, O. T.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 9 p. 934 - 939
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 9 p. 1173 - 1178
反应条件
sodium hydride in 1,4-dioxane 1.) 70 deg C, 1 h 2.) 80 deg C, 16 h;
参考文献
Lukyanenko, N. G.; Melnik, O. T.; Kirichenko, T. I.
Synthesis, 1986 , # 11 p. 930 - 931
反应条件
potassium carbonate in N,N-dimethyl-formamide 16 h; Reflux;
参考文献
Nagarajan, Subbiah; Jeganathan Shanmugam; Mohan Das, Thangamuthu
Carbohydrate Research, 2011 , vol. 346, # 6 p. 722 - 727
反应条件
1: 80 percent / NaN3 / aq. ethanol / 1.)60 deg C, 1 h 2.)reflux, 8-10 h 2: 82 percent / lithium aluminum hydride / tetrahydrofuran / 10 h / Heating 3: 60 percent / toluene / 1.)0 deg C, 7 h 2.)overnight 4: 85 percent / lithium aluminum hydride / tetrahydrofuran / 8 h / Heating View Scheme
参考文献
Gansow, Otto A.; Kausar, A. Rashid; Triplett, Kelly B.
Journal of Heterocyclic Chemistry, 1981 , vol. 18, p. 297 - 302
反应条件
potassium hydroxide; 2,3,11,12-dicyclohexano-1,4,7,10,13,16-hexaoxacyclo-octadecane in tetrahydrofuran 5 h; Heating;
参考文献
Abakumova, N. I.; Kolenko, I. K.; Kodess, M. I.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1305 - 1307
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 7 p. 1495 - 1498
反应条件
sodium hydride 1) THF, 24 h, 2) 96 h; Yield given. Multistep reaction;
参考文献
Keegstra, Erik M. D.; Zwikker, Jan W.; Roest, Martin R.; Jenneskens, Leonardus W.
Journal of Organic Chemistry, 1992 , vol. 57, # 24 p. 6678 - 6680
反应条件
sodium hydride in 1,4-dioxane T=55 - 60°C; 24 h;
参考文献
Samoshin, V. V.; Zelenkina, O. A.; Subbotin, O. A.; Sergeev, N. M.; Zefirov, N. S.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 3 p. 413 - 418
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 3 p. 465 - 471
