三乙二醇二(对甲苯磺酸酯)合成路线 （共 90 条）
反应条件
sodium carbonate in acetonitrile 168 h; Heating;
参考文献
Krakowiak; Bradshaw
Tetrahedron Letters, 1993 , vol. 34, # 5 p. 777 - 778
反应条件
sodium hydride in tetrahydrofuran 1.) 40 min, 2.) 67 deg C, 34 h;
参考文献
Gibson, Harry W.; Bheda, Mukesh C.; Engen, Paul; Shen, Ya Xi; Sze, Jean; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 8 p. 2186 - 2196
反应条件
sodium hydride in tetrahydrofuran 12 h;
参考文献
Beadle, James R.; Khanna, Raj K.; Gokel, George W.
Journal of Organic Chemistry, 1983 , vol. 48, # 8 p. 1242 - 1246
反应条件
cesium fluoride in acetonitrile 24 h; Heating;
参考文献
Lockhart, Joyce C.; McDonnell, Martin B.; Tyson, Philip D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 2153 - 2160
反应条件
potassium hydroxide 1.) 50 deg C, 0.1 mm Hg, 5 h, 2.) THF, room temperature, 10 d; Yield given. Multistep reaction;
参考文献
Yang, Zhuo; Yu, Ga-Er; Cooke, Jennifer; Ali-Adib, Ziad; Viras, Kyriakos; Matsuura, Hiroatsu; Ryan, Anthony J.; Booth, Colin
Journal of the Chemical Society - Faraday Transactions, 1996 , vol. 92, # 17 p. 3173 - 3182
反应条件
1.1: sodium azide; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 16 h / 80 °C 2.1: hydrogenchloride; triphenylphosphine / water; toluene / 16 h / 0 - 20 °C 3.1: triethylamine / dichloromethane / 0.83 h 4.1: triphenylphosphine / tetrahydrofuran / 5 h 4.2: 2 h View Scheme
参考文献
ChemBioChem, , vol. 11, # 12 p. 1769 - 1781
反应条件
1: sodium azide; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 80 °C 2: triphenylphosphine; hydrogenchloride / tetrahydrofuran; diethyl ether / 20 - 22 °C View Scheme
参考文献
Loska, Rafal; Janiga, Anita; Gryko, Dorota
Journal of Porphyrins and Phthalocyanines, 2013 , vol. 17, # 1-2 p. 104 - 117
反应条件
sodium hydroxide; tetra-(n-butyl)ammonium iodide in toluene 16 h; Heating;
参考文献
Bogaschenko, Tatyana; Basok, Stepan; Kulygina, Catherine; Lyapunov, Alexander; Lukyanenko, Nikolay
Synthesis, 2002 , # 15 p. 2266 - 2270
反应条件
potassium hydroxide in ethanol; N,N-dimethyl-formamide; butan-1-ol Heating;
参考文献
Weber, Edwin
Chemische Berichte, 1985 , vol. 118, # 11 p. 4439 - 4452
反应条件
potassium hydroxide 1.) 50 deg C, 0.1 mm Hg, 5 h, 2.) THF, room temperature, 10 d; Yield given. Multistep reaction;
参考文献
Yang, Zhuo; Yu, Ga-Er; Cooke, Jennifer; Ali-Adib, Ziad; Viras, Kyriakos; Matsuura, Hiroatsu; Ryan, Anthony J.; Booth, Colin
Journal of the Chemical Society - Faraday Transactions, 1996 , vol. 92, # 17 p. 3173 - 3182
