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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
19253-17-9
合成路线
（共 5 条）
130471-80-6
→
反应条件
19253-17-9
反应条件
hydrogen; palladium on activated charcoal in methanol P=760 Torr; 100 h;
参考文献
Esaki, Sachiko; Abe, Manami; Shiba, Naoko; Kamiya, Shintaro
Agricultural and Biological Chemistry, 1990 , vol. 54, # 6 p. 1583 - 1585
130471-75-9
→
反应条件
19253-17-9
反应条件
1: 37.8 percent / mercuric cyanide, nitromethane / Heating 2: 0.1 N NaOMe / methanol / 2 h / Ambient temperature 3: 41.4 percent / KOH / ethanol / 96 h / Ambient temperature 4: 70.6 percent / H2 / 10 percent Pd/C / methanol / 100 h / 760 Torr View Scheme
参考文献
Esaki, Sachiko; Abe, Manami; Shiba, Naoko; Kamiya, Shintaro
Agricultural and Biological Chemistry, 1990 , vol. 54, # 6 p. 1583 - 1585
130471-77-1
→
反应条件
19253-17-9
反应条件
1: 0.1 N NaOMe / methanol / 2 h / Ambient temperature 2: 41.4 percent / KOH / ethanol / 96 h / Ambient temperature 3: 70.6 percent / H2 / 10 percent Pd/C / methanol / 100 h / 760 Torr View Scheme
参考文献
Esaki, Sachiko; Abe, Manami; Shiba, Naoko; Kamiya, Shintaro
Agricultural and Biological Chemistry, 1990 , vol. 54, # 6 p. 1583 - 1585
130471-78-2
→
反应条件
19253-17-9
反应条件
1: 41.4 percent / KOH / ethanol / 96 h / Ambient temperature 2: 70.6 percent / H2 / 10 percent Pd/C / methanol / 100 h / 760 Torr View Scheme
参考文献
Esaki, Sachiko; Abe, Manami; Shiba, Naoko; Kamiya, Shintaro
Agricultural and Biological Chemistry, 1990 , vol. 54, # 6 p. 1583 - 1585
5160-09-8
→
反应条件
19253-17-9
反应条件
1: 37.8 percent / mercuric cyanide, nitromethane / Heating 2: 0.1 N NaOMe / methanol / 2 h / Ambient temperature 3: 41.4 percent / KOH / ethanol / 96 h / Ambient temperature 4: 70.6 percent / H2 / 10 percent Pd/C / methanol / 100 h / 760 Torr View Scheme
参考文献
Esaki, Sachiko; Abe, Manami; Shiba, Naoko; Kamiya, Shintaro
Agricultural and Biological Chemistry, 1990 , vol. 54, # 6 p. 1583 - 1585
