6-氨基己酸甲酯 盐酸盐合成路线 （共 21 条）
反应条件
hydrogen chloride (gas) in methanol
参考文献
Neorx Corporation
Patent: US5578287 A1, 1996 ;
反应条件
hydrogenchloride T=20°C; 10 h;
参考文献
Niimi; Orita; Okazawa-Igarashi; Sakashita; Kikuchi; Ball; Ichikawa; Yamagiwa; Sakamoto; Tanaka; Tsukamoto; Fujita
Journal of Medicinal Chemistry, 2001 , vol. 44, # 26 p. 4737 - 4740
反应条件
hydrogenchloride in water T=20°C; 18 h;
参考文献
Zlatev, Ivan; Dutartre, Helene; Barvik, Ivan; Neyts, Johan; Canard, Bruno; Vasseur, Jean-Jacques; Alvarez, Karine; Morvan, Francois
Journal of Medicinal Chemistry, 2008 , vol. 51, # 18 p. 5745 - 5757
反应条件
hydrogenchloride in 1,4-dioxane 0.5 h; Ambient temperature;
参考文献
Paruszewski, Ryszard; Matusiak, Roza; Rostafinska-Suchar, Grazyna; Gumulka, Stanislaw; Misterek, Krystyna; Dorociak, Anna
Polish Journal of Chemistry, 1991 , vol. 65, # 2-3 p. 361 - 368
反应条件
1: 98 percent / NaHCO3 / dimethylformamide / 120 h / Ambient temperature 2: 98 percent / HCl / dioxane / 0.5 h / Ambient temperature View Scheme
参考文献
Polish Journal of Chemistry, , vol. 65, # 2-3 p. 361 - 368
反应条件
1: 940 mg / NaHCO3 / methanol / 24 h 2: 325 mg / NaOH / H2O; tetrahydrofuran / 3 h / 20 °C View Scheme
参考文献
Wender, Paul A.; Baryza, Jeremy L.
Organic Letters, 2005 , vol. 7, # 6 p. 1177 - 1180
反应条件
1: 74 percent / Et3N / dimethylformamide 2: 85 percent / 1 M NaOH / methanol; H2O / 20 °C View Scheme
参考文献
Schoen, Istvan; Nyeki, Olga; Demeter, Adam
Journal of Labelled Compounds and Radiopharmaceuticals, 2000 , vol. 43, # 4 p. 309 - 322
反应条件
sodium carbonate; benzenesulfonyl chloride in water; acetonitrile
参考文献
Watkins, Clare; Romero-Martin, Maria Rosario; Moore, Kathryn G; Ritchie, James; Finn, Paul W; Kalvinsh, Ivars; Loza, Einars; Dikovska, Klara; Gailite, Vija; Vorona, Maxim; Piskunova, Irina; Starchenkov, Igor; Andrianov, Victor; Harris, C. John; Duffy, James E.S.
Patent: US2004/77726 A1, 2004 ;
反应条件
1: ethanol; sodium acetate View Scheme
参考文献
Plit; Burmistrow
Ukrainskii Khimicheskii Zhurnal (Russian Edition), 1958 , vol. 24, p. 73
Chem.Abstr., 1958 , p. 18271
反应条件
dichloromethane; chloroform; triethylamine Reagens 4: Chlorokohlensaeure-aethylester;
参考文献
Garmaise et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 3332
