1-苄基-2-氯甲基-咪唑盐酸盐合成路线 (共 7 条)
反应条件
thionyl chloride in chloroform 2 h; Heating;
参考文献
Birker, Paul J. M. W. L.; Godefroi, Eric F.; Helder, Janneke; Reedijk, Jan
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7556 - 7560
反应条件
1: 56 percent / H2O / 72 h / Heating 2: 95 percent / SOCl2 / CHCl3 / 2 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 104, # 26 p. 7556 - 7560
反应条件
thionyl chloride 0.5 h; Ambient temperature;
参考文献
Synthesis, , # 12 p. 1103 - 1105
参考文献
Durant et al.
Chemical Communications (London), 1968 , p. 108
反应条件
in methanol; dimethyl sulfoxide
参考文献
Merck and Co., Inc.
Patent: US4746669 A1, 1988 ;
反应条件
1: 97 percent / dimethylformamide / 1 h / 80 °C
2: 85 percent / aq. NaOH / 1.17 h / Heating
3: 44 percent / ethanol / 4.5 h / Heating
View Scheme
参考文献
Birker, Paul J. M. W. L.; Godefroi, Eric F.; Helder, Janneke; Reedijk, Jan
Journal of the American Chemical Society, 1982 , vol. 104, # 26 p. 7556 - 7560
反应条件
sodium ethanolate in ethanol
参考文献
Galley, Guido; Zbinden, Katrin Groebke; Hoener, Marius; Kolczewski, Sabine; Norcross, Roger; Stalder, Henri
Patent: US2007/197621 A1, 2007 ;
Location in patent: Page/Page column 59-60 ;
US 20070197621 A1