2,4-二氯苯氧乙酸甲酯合成路线 （共 10 条）
反应条件
1: dimethylammonium 2,4-dichlorophenoxyacetate in sodium hydroxide T=80°C; Hydrolysis; pH=14; 0.333333 h; 2: methanol; [3H]-2,4-Dichlorophenoxyacetic acid; (BF3)-MeOH complex in diethyl ether Esterification; pH=2; Heating;
参考文献
Lin; Que Hee
Archives of Environmental Contamination and Toxicology, 1999 , vol. 36, # 4 p. 485 - 489
反应条件
in water T=45°C; 730.5 h; Emulsifier; Reactivity;
参考文献
US2007/184980 A1, ;
Page/Page column 2-3 ;
反应条件
1: [3H]-2,4-Dichlorophenoxyacetic acid With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=20°C; 0.5 h; 2: methanol With sodium tetrahydroborate in tetrahydrofuran T=0°C; 0.5 h;
参考文献
Synthesis, , # 9 art. no. M12811SS, p. 1375 - 1382
反应条件
toluene-4-sulfonic acid Abdestillieren des entstehenden Wassers;
参考文献
Journal of the American Chemical Society, , vol. 69, p. 718,721
反应条件
AG-MP1 anion exchange resin in carbon dioxide T=80°C; P=150012 Torr; 0.333333 h; Product distribution;
参考文献
Chatfield; Croft; Dang; Murby; Yu; Wells
Analytical Chemistry, 1995 , vol. 67, # 5 p. 945 - 951
反应条件
1: Weedar Brand 64; emulsion of in sodium hydroxide T=80°C; Hydrolysis; pH=14; 0.333333 h; 2: methanol; [3H]-2,4-Dichlorophenoxyacetic acid; (BF3)-MeOH complex in diethyl ether Esterification; pH=2; Heating;
参考文献
Archives of Environmental Contamination and Toxicology, , vol. 36, # 4 p. 485 - 489
反应条件
potassium carbonate; potassium iodide; PEG-600 in N,N-dimethyl-formamide 0.0666667 h; microwave irradiation;
参考文献
Journal of Chemical Research, , # 7 p. 432 - 433
反应条件
1: N2H4*H2O / ethanol / Heating 2: ethanol / Heating View Scheme
参考文献
Ram; Pandey
Chemical and Pharmaceutical Bulletin, 1974 , vol. 22, # 12 p. 2778 - 2783
反应条件
hydrazine hydrate in ethanol Heating;
参考文献
Wei, Tai-Bao; Liu, Hong; Li, Man-Lin; Zhang, You-Ming
Journal of Chemical Research, 2005 , # 7 p. 432 - 433
反应条件
(i) aq. NH3, (ii) P2S5, benzene; Multistep reaction;
参考文献
Abdel-Lateef,M.F.-A.; Eckstein,Z.
Bulletin de l'Academie Polonaise des Sciences, Serie des Sciences Chimiques, 1971 , vol. 19, # 11-12 p. 705 - 711
