100°C; starting mixt. of 52.5 percent B2H6 and 47.5 percent HCl; 740 Torr; 30 h;
参考文献
Cueilleron, J.; Reymonet, J. L.
Bulletin de la Societe Chimique de France, 1967 , p. 1370 - 1374
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Gmelin Handbook: B: B-Verb.9, 1.2.2.1, page 15 - 20
Burg, A. B.; Randolph, C. L.
Journal of the American Chemical Society, 1951 , vol. 73, p. 953 - 957
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Gmelin Handbook: B: B-Verb.4, 3.2, page 41 - 51
in pentane
B2H6 was condensed at -193 °C to the soln. of the borolidine, then the mixture was warmed up to -60 °C; the product was sepd., washed with cold pentane;
参考文献
Anton, Klaus; Noeth, Heinrich; Pommerening, Hans
Chemische Berichte, 1984 , vol. 117, # 7 p. 2479 - 2494
Keller, P. C.
Inorganic Chemistry, 1971 , vol. 10, p. 1528 - 1529
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Gmelin Handbook: B: B-Verb.8, 10.2, page 150 - 154
Wiberg, E.; Bolz, A.; Buchheit, P.
Z. Anorg. Chem., 1948 , vol. 256, p. 285 - 306
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Gmelin Handbook: B: SVol.1, 4.10, page 238 - 241