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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
192887-50-6
合成路线
（共 21 条）
17763-67-6
苯基三氟甲烷磺酸酯
+
192887-50-6
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
1: p-MeOC6H4MnCl With IPr*hydrochloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=0°C; 0.5 h; 2: trifluoromethanesulfonyloxybenzene in tetrahydrofuran T=0 - 25°C; 5 h;
参考文献
Leleu, Anne; Fort, Yves; Schneider, Raphael
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 9 p. 1086 - 1092
108-90-7
氯苯
+
192887-50-6
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
1: p-MeOC6H4MnCl With IPr*hydrochloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=0°C; 0.5 h; 2: chlorobenzene in tetrahydrofuran T=0 - 25°C; 7 h;
参考文献
Leleu, Anne; Fort, Yves; Schneider, Raphael
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 9 p. 1086 - 1092
640-60-8
对甲苯亚磺酸苯酯
+
192887-50-6
→
反应条件
613-37-6
4-甲氧基联苯
+
53040-92-9
4-甲氧基-4-甲基-联苯
反应条件
1: p-MeOC6H4MnCl With IPr*hydrochloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=0°C; 0.5 h; 2: p-toluenesulfonyloxybenzene in tetrahydrofuran T=0 - 25°C; 15 h;
参考文献
Advanced Synthesis and Catalysis, , vol. 348, # 9 p. 1086 - 1092
100-47-0
苯甲腈
+
192887-50-6
→
反应条件
613-37-6
4-甲氧基联苯
反应条件
[NiCl2(PMe3)2] in tetrahydrofuran T=70°C; 12 h; Inert atmosphere;
参考文献
Liu, Ning; Wang, Zhong-Xia
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 9 p. 1641 - 1645
591-17-3
3-溴甲基苯
+
192887-50-6
→
反应条件
17171-17-4
4-甲氧基-3-甲基联苯
反应条件
1: p-MeOC6H4MnCl With IPr*hydrochloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=0°C; 0.5 h; 2: 1-bromo-3-methyl-benzene in tetrahydrofuran T=0 - 25°C; 11 h;
参考文献
Leleu, Anne; Fort, Yves; Schneider, Raphael
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 9 p. 1086 - 1092
90-90-4
4-溴苯甲酰苯
+
192887-50-6
→
反应条件
68294-33-7
(4-甲氧基联苯-4-基)-苯基-甲酮
反应条件
1: p-MeOC6H4MnCl With IPr*hydrochloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=0°C; 0.5 h; 2: (4-bromophenyl)(phenyl)methanone in tetrahydrofuran T=0 - 25°C; 13 h;
参考文献
Leleu, Anne; Fort, Yves; Schneider, Raphael
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 9 p. 1086 - 1092
95-46-5
邻溴甲苯
+
192887-50-6
→
反应条件
92495-54-0
4-甲氧基-2-甲基-联苯
反应条件
1: p-MeOC6H4MnCl With IPr*hydrochloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=0°C; 0.5 h; 2: 1-bromo-2-methyl benzene in tetrahydrofuran T=0 - 25°C; 24 h;
参考文献
Leleu, Anne; Fort, Yves; Schneider, Raphael
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 9 p. 1086 - 1092
402-43-7
对溴三氟甲苯
+
192887-50-6
→
反应条件
10355-12-1
反应条件
1: p-MeOC6H4MnCl With IPr*hydrochloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=0°C; 0.5 h; 2: 1-trifluoromethyl-4-bromobenzene in tetrahydrofuran T=0 - 25°C; 7 h;
参考文献
Leleu, Anne; Fort, Yves; Schneider, Raphael
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 9 p. 1086 - 1092
98-56-6
对氯三氟甲苯
+
192887-50-6
→
反应条件
10355-12-1
反应条件
1: p-MeOC6H4MnCl With IPr*hydrochloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=0°C; 0.5 h; 2: 1-chloro-4-(trifluoromethyl)benzene in tetrahydrofuran T=0 - 25°C; 15 h;
参考文献
Leleu, Anne; Fort, Yves; Schneider, Raphael
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 9 p. 1086 - 1092
109-04-6
邻溴吡啶
+
192887-50-6
→
反应条件
5957-90-4
4-(2-吡啶基)苯甲醚
反应条件
1: p-MeOC6H4MnCl With IPr*hydrochloride; bis(acetylacetonate)nickel(II) in tetrahydrofuran T=0°C; 0.5 h; 2: 2-bromo-pyridine in tetrahydrofuran T=0 - 25°C; 1 h;
参考文献
Leleu, Anne; Fort, Yves; Schneider, Raphael
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 9 p. 1086 - 1092
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