3-(4-甲氧基苯基)丙酸合成路线 （共 94 条）
反应条件
carbon monoxide; palladium on activated charcoal; 1,4-di(diphenylphosphino)-butane in ethylene glycol dimethyl ether T=150°C; P=30400 Torr; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 58, # 17 p. 4739 - 4741
反应条件
hydrogenchloride; oxygen; 6-hydroxy-6-oxo-2,5,7,10-tetraoxa-6-phospha-tricyclo[6.3.0.04,11]undecane; copper dichloride; palladium dichloride in tetrahydrofuran; water T=20°C; 12 h; Title compound not separated from byproducts;
参考文献
Heterocycles, , vol. 63, # 12 p. 2797 - 2803
反应条件
sodium hydroxide in methanol T=50°C; 10 h;
参考文献
Kawasaki, Masashi; Goto, Michimasa; Kawabata, Shigeki; Kometani, Tadashi
Tetrahedron Asymmetry, 2001 , vol. 12, # 4 p. 585 - 596
反应条件
1: 94 percent / tetrahydrofuran / 4 h / Heating 2: 99 percent / H2 / 10percent Pd/C / ethanol / 1 h / 25 °C / 2327.2 Torr 3: 94 percent / water, KOH / methanol / 2 h / 25 °C View Scheme
参考文献
Synthetic Communications, , vol. 21, # 21 p. 2231 - 2256
反应条件
1: With sodium hydroxide in ethanol 2: With hydrogenchloride in water
参考文献
Mimori, Seisuke; Okuma, Yasunobu; Kaneko, Masayuki; Kawada, Koichi; Nomura, Yasuyuki; Murakami, Yasuoki; Hamana, Hiroshi
Chemistry Letters, 2013 , vol. 42, # 9 p. 1051 - 1052
反应条件
[Rh(OH)(cycloocta-1,5-diene)]2; water T=75°C; Miyaura-Hayashi reaction; 16 h; Inert atmosphere;
参考文献
Vautravers, Nicolas R.; Breit, Bernhard
Synlett, 2011 , # 17 p. 2517 - 2520
反应条件
1: AlCl3; carbon disulfide 2: sulfur; benzene / 135 °C 3: aq.-ethanolic KOH-solution View Scheme
参考文献
Chemische Berichte, , vol. 74, p. 321,324
反应条件
1: 99 percent / H2 / 10percent Pd/C / ethanol / 1 h / 25 °C / 2327.2 Torr 2: 94 percent / water, KOH / methanol / 2 h / 25 °C View Scheme
参考文献
Synthetic Communications, , vol. 21, # 21 p. 2231 - 2256
反应条件
1: aqueous NaOH View Scheme
参考文献
Journal of the American Chemical Society, , vol. 76, p. 1076,1077
反应条件
1.1: n-BuLi; NaH / tetrahydrofuran; hexane / 0.33 h / 0 °C 1.2: tetrahydrofuran; hexane / 2 h 2.1: 81 percent / ceric ammonium nitrate / acetonitrile / 4 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 71, # 12 p. 4516 - 4520
