1,3-二苯基丙烷-1,3-二胺合成路线 （共 6 条）
反应条件
1: Py / ethanol 2: (i) B2H6, THF, (ii) aq. KOH View Scheme
参考文献
Feuer,H.; Braunstein,D.M.
Journal of Organic Chemistry, 1969 , vol. 34, # 6 p. 1817 - 1821
反应条件
potassium hydroxide in ethanol
参考文献
Merten,R.; Mueller,G.
Angewandte Chemie, 1962 , vol. 74, p. 866 - 871
反应条件
1,4-dioxane; nickel Hydrogenation;
参考文献
Samne
Annales de Chimie (Cachan, France), 1957 , vol. <13>2, p. 629,643
反应条件
(i) B2H6, THF, (ii) aq. KOH; Multistep reaction;
参考文献
Feuer,H.; Braunstein,D.M.
Journal of Organic Chemistry, 1969 , vol. 34, # 6 p. 1817 - 1821
反应条件
1: iodine; potassium carbonate / tert-butyl alcohol
2: pyridine / dichloromethane / 0 - 20 °C
3: sodium hydroxide / dimethyl sulfoxide / 4 h / 60 °C
View Scheme
参考文献
Trieu, Tien Ha; Dong, Jing; Shi, Xiao-Xin; Lu, Xia; Zhang, Qiang
Synthetic Communications, 2013 , vol. 43, # 23 p. 3141 - 3152
反应条件
1: iodine; potassium carbonate / tert-butyl alcohol
2: pyridine / dichloromethane / 0 - 20 °C
3: sodium hydroxide / dimethyl sulfoxide / 4 h / 60 °C
View Scheme
参考文献
Trieu, Tien Ha; Dong, Jing; Shi, Xiao-Xin; Lu, Xia; Zhang, Qiang
Synthetic Communications, 2013 , vol. 43, # 23 p. 3141 - 3152
