3,5-二(溴甲基)甲苯合成路线 （共 14 条）
反应条件
N-bromosuccinmide; dibenzoyl peroxide in benzene T=85°C; 12 h;
参考文献
Lee, Insuk; You, Ngmin; Lim, Seon-Jeong; Park, Soo Young
Chemistry Letters, 2007 , vol. 36, # 7 p. 888 - 889
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in cyclohexane 0.5 h; Heating / reflux; Product distribution / selectivity;
参考文献
HELM AG
Patent: US2006/217569 A1, 2006 ;
Location in patent: Page/Page column 3; 4 ;
参考文献
Bulletin de la Societe Chimique de France, , vol. <2> 40, p. 110
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile; dibenzoyl peroxide in tetrachloromethane Heating;
参考文献
Tetrahedron, , vol. 25, p. 2349 - 2365
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 3 h; Heating; Title compound not separated from byproducts;
参考文献
Dalton Transactions, , # 42 p. 4996 - 5013
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; acetic acid 1.) chloroform, reflux, 1 h, 0 deg C, 3 h; 2.) water, reflux, 1 h; Yield given. Multistep reaction;
参考文献
Chan, Tze-Lock; Mak, Thomas C. W.; Trotter, James
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 672 - 675
反应条件
1: tetrachloromethane; dibenzoyl peroxide; <α,α'>azoisobutyronitrile; N-bromo-succinimide 2: methanol / Behandeln der Reaktionsloesung mit warmer wss. Natriumperchlorat-Loesung 3: N,N-dimethyl-4-nitroso-aniline / Hydrolysieren des Reaktionsprodukts View Scheme
参考文献
Ried; Koenigstein
Chemische Berichte, 1959 , vol. 92, p. 2532,2538
反应条件
tetrabutylammomium bromide in dichloromethane; water 8 - 9 h; Heating / reflux;
参考文献
US2006/189670 A1, ;
Page/Page column 5-6 ;
反应条件
tetrabutylammomium bromide in dichloromethane; water
参考文献
US4935437 A1, ;
US 4935437 A
反应条件
tetrabutylammomium bromide in dichloromethane; water 16 h; Heating;
参考文献
Organic and Biomolecular Chemistry, , vol. 5, # 18 p. 2940 - 2952
