[1,3-亚苯基二(亚甲基)]二(二异丙基膦)合成路线 （共 3 条）
反应条件
1: in methanol T=50°C; 48 h; 2: With triethylamine in methanol T=20°C; 0.5 h; Further stages.;
参考文献
Montag, Michael; Schwartsburd, Leonid; Cohen, Revital; Leitus, Gregory; Ben-David, Yehoshoa; Martin, Jan M. L.; Milstein, David
Angewandte Chemie - International Edition, 2007 , vol. 46, # 11 p. 1901 - 1904
反应条件
in toluene T=100°C; 18 h; Inert atmosphereSchlenk technique;
参考文献
Vabre, Boris; Lambert, Melinda L.; Petit, Alban; Ess, Daniel H.; Zargarian, Davit
Organometallics, 2012 , vol. 31, # 17 p. 6041 - 6053
反应条件
in tetrahydrofuran
byproducts: PPh3; stirring (110°C, 10 h); filtering, washing (pentane, -30°C), drying (vac.); elem. anal.;
参考文献
Van Der Boom, Milko E.; Kraatz, Heinz-Bernhard; Hassner, Lawrence; Ben-David, Yehoshoa; Milstein, David
Organometallics, 1999 , vol. 18, # 19 p. 3873 - 3884
