1: 4.7 g / 3 h / 0 °C
2: 1.5 g / hydrogen / Lindlar catalyst / ethyl acetate
3: 330 mg / pyridinium chlorochromate / CH2Cl2 / 6 <unit not given> / 20 °C
4: sodium borohydride / methanol
View Scheme
参考文献
Frankel, Edwin N.; Garwood, Robert F.; Khambay, Bhupinder P. S.; Moss, Gerard P.; Weedon, Basil C. L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 10 p. 2233 - 2240
1: diethyl ether / -10 °C
2: PBr3 / beim nachfolgenden Kochen des Bromderivats mit alkoh.KOH und Hydrieren an Platinoxyd in Aethanol bei 2-3 at
View Scheme
参考文献
Fordyce; Johnson
Journal of the American Chemical Society, 1933 , vol. 55, p. 3371