3-氯-N-(4-甲氧基苯基)丙酰胺合成路线 （共 9 条）
反应条件
potassium carbonate in acetone T=0°C; Condensation; 1 h;
参考文献
Chen, I.-Li; Wang, Tai-Chi; Chen, Yeh-Long; Tzeng, Cherng-Chyi
Journal of the Chinese Chemical Society, 2000 , vol. 47, # 1 p. 155 - 162
反应条件
in N,N-dimethyl-formamide
参考文献
Mendelovici, Marioara; Pilarsky, Gideon; Nidam, Tamar; Dolitzky, Ben-Zion
Patent: US2002/32333 A1, 2002 ;
反应条件
in benzene Ambient temperature;
参考文献
Die Pharmazie, , vol. 23, # 10 p. 561 - 566
反应条件
sodium borohydride in hydrogenchloride; N,N-dimethyl acetamide; water
参考文献
Mendelovici, Marioara; Pilarsky, Gideon; Nidam, Tamar; Dolitzky, Ben-Zion
Patent: US2002/32333 A1, 2002 ;
反应条件
aluminium trichloride in chlorobenzene T=120°C; Cyclization; 6 h;
参考文献
Chen, I.-Li; Wang, Tai-Chi; Chen, Yeh-Long; Tzeng, Cherng-Chyi
Journal of the Chinese Chemical Society, 2000 , vol. 47, # 1 p. 155 - 162
反应条件
1.1: AlCl3, aluminium chloride / N,N-dimethyl acetamide / 140 - 150 °C
2.1: potassium carbonate / water; acetone / 1 h / 20 °C
2.2: 16 h / 20 °C
View Scheme
参考文献
Pai; Samel
Asian Journal of Chemistry, 2011 , vol. 23, # 4 p. 1655 - 1660
反应条件
potassium hydroxide; p-tert-butylcalixlt;4gt;arene tetraamide in dichloromethane; acetonitrile
0.5 h;
参考文献
Harris, Stephen J.; Kinahan, Audrey M.; Meegan, Mary J.; Prendergast, Rhona C.
Journal of Chemical Research, Miniprint, 1994 , # 9 p. 1832 - 1845
反应条件
potassium tert-butylate in tetrahydrofuran
T=0°C; 2 h;
参考文献
Wang, Eng Chi; Lin, Huey-Jen
Heterocycles, 1998 , vol. 48, # 3 p. 481 - 489
反应条件
potassium tert-butylate in tetrahydrofuran
T=25 - 30°C;
参考文献
Wang, Eng Chi; Lin, Huey-Jen
Heterocycles, 1998 , vol. 48, # 3 p. 481 - 489
