1: Pd(OAc)2 2: 0.3 percent Chromat. / HBF4 / acetonitrile / 2.03 h / 25 °C View Scheme
参考文献
Ikenaga, Kazutoshi; Kikukawa, Kiyoshi; Matsuda, Tsutomu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1959 - 1964
bis(dibenzylideneacetone)-palladium(0) in acetonitrile T=25°C; Yield given. Yields of byproduct given;
参考文献
Ikenaga, Kazutoshi; Kikukawa, Kiyoshi; Matsuda, Tsutomu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1959 - 1964
1: With diisobutylaluminium hydride in diethyl ether; hexane
T=20°C; 50.1667 h; Inert atmosphere;
2: With sulfuric acid in diethyl ether; hexane; water
stereoselective reaction;
参考文献
Sheshenev, Andrey E.; Baird, Mark S.; Bolesov, Ivan G.; Shashkov, Alexandre S.
Tetrahedron, 2009 , vol. 65, # 51 p. 10552 - 10564
molecular sieve; tris(dimethylamino)-sulphonium difluorotrimethylsilicate in tetrahydrofuran
T=70°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Palomo, Claudio; Aizpurua, Jesus M.; Garcia, Jesus M.; Ganboa, Inaki; Cossio, F. P.; et al.
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2498 - 2503
