1: 85 percent / hydrogen / 5percent Pd-C / methanol / 6 h / Ambient temperature 2: 41 percent / PCl5 / benzene / 4 h / Heating 3: 95 percent / SOCl2 / CHCl3; dimethylformamide / 1 h / Heating; other reagent (PCl5/POCl3); other solvent (neat) View Scheme

hydrogen; palladium on activated charcoal in methanol 6 h; Ambient temperature;

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<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '605283', constants.ctx, '0')">triethylamine</a> <br /> <br /> &nbsp;