(1R,3S)-1,2,2-三甲基-1,3-环戊烷二羰基二氟化物合成路线 (共 3 条)
反应条件
sulfur(IV) fluoride T=25°C; 0.5 h; Yields of byproduct given;
参考文献
Dmowski, Wojciech; Kozlowski, Tomasz
Journal of Fluorine Chemistry, 1997 , vol. 83, # 2 p. 187 - 190
反应条件
1: With sulfur(IV) fluoride T=20 - 25°C; Fluorination; 240 h; 2: With potassium hydroxide; water T=20°C; Hydrolysis; Title compound not separated from byproducts;
参考文献
Dmowski, Wojciech; Piasecka-Maciejewska, Krystyna
Organic Preparations and Procedures International, 1999 , vol. 31, # 2 p. 207 - 211
反应条件
sulfur(IV) fluoride T=20 - 25°C; Fluorination; 240 h; Title compound not separated from byproducts;
参考文献
Dmowski, Wojciech; Piasecka-Maciejewska, Krystyna
Organic Preparations and Procedures International, 1999 , vol. 31, # 2 p. 207 - 211