trimethylsilylazide; boron trifluoride diethyl etherate in dichloromethane
T=-78°C;
参考文献
Takeuchi, Hisato; Eguchi, Shoji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2149 - 2154
1: 81 percent / tetrahydrofuran; diethyl ether / 3 h / Ambient temperature
2: 52 percent / trimethylsilyl azide, BF3.Et2O / CH2Cl2 / -78 °C
View Scheme
参考文献
Takeuchi, Hisato; Eguchi, Shoji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2149 - 2154