2-[(4-甲氧基苯基)氨基]-1,2-二苯基-乙酮合成路线 （共 8 条）
反应条件
TiI4 in acetonitrile
T=0 - 20°C; 30 h;
参考文献
Shimizu, Makoto; Sahara, Tetsuya; Hayakawa, Ryuuichirou
Chemistry Letters, 2001 , # 8 p. 792 - 793
反应条件
dicobalt octacarbonyl in tetrahydrofuran
T=60°C; P=760 Torr; 24 h;
参考文献
Alper, Howard; Amaratunga, Shiyamalie
Journal of Organic Chemistry, 1982 , vol. 47, # 18 p. 3593 - 3595
反应条件
hydrogenchloride in water
T=140°C; 3 h;
参考文献
Van Belzen, Ruud; Klein, Rene A.; Smeets, Wilberth J.J.; Spek, Anthony L.; Benedix, Roland; Elsevier, Cornelis J.
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, 1996 , vol. 115, # 5 p. 275 - 285
反应条件
in tetrahydrofuran
T=60°C; 7 h;
参考文献
Alper, Howard; Amaratunga, Shiyamaline
Tetrahedron Letters, 1981 , vol. 22, # 39 p. 3811 - 3812
反应条件
1: 80 percent / ZnCl2-1-phenylethylamine complex / xylene / 6 h
2: 76 percent / H2 / Pd(C) / ethyl acetate / 0.5 h / Ambient temperature
View Scheme
参考文献
Alcaide, Benito; Lopez-Mardomingo, Carmen; Perez-Ossorio, Rafael; Plumet, Joaquin
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 11 p. 1649 - 1654
反应条件
1: 80 percent / ZnCl2-1-phenylethylamine complex / xylene / 6 h
2: 76 percent / H2 / Pd(C) / ethyl acetate / 0.5 h / Ambient temperature
View Scheme
参考文献
Alcaide, Benito; Lopez-Mardomingo, Carmen; Perez-Ossorio, Rafael; Plumet, Joaquin
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , # 11 p. 1649 - 1654
反应条件
1: cyclopentyl-magnesium chloride / diethyl ether / 1.5 h / -30 °C / |Schlenk technique; |Inert atmosphere
2: 3 h / -30 °C / |Schlenk technique; |Inert atmosphere
3: hydrogenchloride; water / 0.5 h / 20 °C / |Schlenk technique; |Inert atmosphere
View Scheme
参考文献
Chen, Haoyi; Fan, Guoqin; Li, Shi; Mao, Kebin; Liu, Yuanhong
Tetrahedron Letters, 2014 , vol. 55, # 9 p. 1593 - 1596
反应条件
potassium hexacyanoferrate(III) in ethanol; water; benzene
T=70°C; 3.5 h;
参考文献
Van Belzen, Ruud; Klein, Rene A.; Smeets, Wilberth J.J.; Spek, Anthony L.; Benedix, Roland; Elsevier, Cornelis J.
Recueil des Travaux Chimiques des Pays-Bas-Journal of the Royal Netherlands, 1996 , vol. 115, # 5 p. 275 - 285
