N-甲基-N-苯基苯甲酰胺合成路线 (共 96 条)
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate in benzene
T=30 - 35°C; 4 h;
参考文献
Ayyangar, N. R.; Choudhary, A. R.; Kalkote, U. R.; Natu, A. A.
Synthetic Communications, 1988 , vol. 18, # 16-17 p. 2011 - 2016
反应条件
PdCl2(PMePh2)2 in neat (no solvent)
T=100°C; P=7600 Torr; 2 h;
参考文献
Ozawa, Fumiyuki; Soyama, Hidehiko; Yanagihara, Hisayoshi; Aoyama, Issei; Takino, Hiroaki; et al.
Journal of the American Chemical Society, 1985 , vol. 107, # 11 p. 3235 - 3245
反应条件
triethylsilane; 2,2-bis(tert-butylperoxy)butane in benzene
T=135°C; 4 h; Inert atmosphere; chemoselective reaction;
参考文献
The Florida State University Research Foundation, Inc.
Patent: US2011/237798 A1, 2011 ;
Location in patent: Page/Page column 13 ;
反应条件
[(Ph3P)2]Ni(CO)2 in benzene
T=180°C; P=30400 Torr; 6 h;
参考文献
Giannoccaro, Potenzo; Pannacciulli, Emiliano
Journal of Organometallic Chemistry, 1987 , vol. 319, p. 119 - 128
反应条件
pyridine; water; methyllithium in diethyl ether; hexane
参考文献
Beak, Peter; Basha, Anwer; Kokko, Bruce; Loo, DeKai
Journal of the American Chemical Society, 1986 , vol. 108, # 19 p. 6016 - 6023
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate in benzene
T=30 - 35°C; 2.5 h;
参考文献
Ayyangar, N. R.; Choudhary, A. R.; Kalkote, U. R.; Natu, A. A.
Synthetic Communications, 1988 , vol. 18, # 16-17 p. 2011 - 2016
反应条件
peroxymonosulfuric acid; silica gel in acetonitrile
T=40°C; Oxidation; 6 h;
参考文献
Movassagh; Lakouraj; Ghodrati
Synthetic Communications, 2000 , vol. 30, # 13 p. 2353 - 2358
反应条件
copper(l) chloride in chlorobenzene
T=130°C; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Xia, Qinqin; Liu, Xiaolong; Zhang, Yuejiao; Chen, Chao; Chen, Wanzhi
Organic Letters, 2013 , vol. 15, # 13 p. 3326 - 3329
反应条件
tris(N-2',6'-diisopropylphenyl(naphthyl)amidate)yttrium mono(tetrahydrofurane) in toluene
T=20°C; 0.0833333 h; Inert atmosphere;
参考文献
Thomson, Jaclyn A.; Schafer, Laurel L.
Dalton Transactions, 2012 , vol. 41, # 26 p. 7897 - 7904
反应条件
tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide in water; 1,2-dichloro-ethane
T=90°C; 10 h;
参考文献
Mai, Wen-Peng; Song, Ge; Yuan, Jin-Wei; Yang, Liang-Ru; Sun, Gang-Chun; Xiao, Yong-Mei; Mao, Pu; Qu, Ling-Bo
RSC Advances, 2013 , vol. 3, # 12 p. 3869 - 3872