N-甲基-N-苯基苯甲酰胺合成路线 (共 96 条)
反应条件
palladium in ethylene glycol dimethyl ether; benzene
T=35 - 40°C; 2 h;
参考文献
Wakita, Yoshiaki; Noma, Shun-Ya; Maeda, Minoru; Kojima, Masaharu
Journal of Organometallic Chemistry, 1985 , vol. 297, p. 379 - 390
反应条件
1: N-methylaniline With isopropylmagnesium chloride lithium chloride complex in tetrahydrofuran
T=20°C; 0.1 h; Microreactor;
2: benzoic acid ethyl ester in tetrahydrofuran
T=20°C; Bodroux reaction; 0.233333 h; Microreactor;
参考文献
Munoz, Juan De M.; Alcazar, Jesus; De La Hoz, Antonio; Diaz-Ortiz, Angel; Alonso De Diego, Sergio-A.
Green Chemistry, 2012 , vol. 14, # 5 p. 1335 - 1341
反应条件
triethylamine in dichloromethane
参考文献
THE GOVERNORS OF THE UNIVERSITY OF ALBERTA; Bergens, Steven; John, Jeremy M.
Patent: US2014/163225 A1, 2014 ;
Location in patent: Page/Page column ;
反应条件
bisallyl ether; triphenylphosphine in 1,4-dioxane
T=18 - 20°C; 5 h;
参考文献
Parfenov, E. A.; Fomin, V. A.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 5 p. 1144 - 1153,961 - 968
反应条件
pyridine; tert.-butylhydroperoxide; iron(II) chloride in acetonitrile
T=85°C; 2 h; Inert atmosphere;
参考文献
Li, Yuanming; Ma, Lina; Jia, Fan; Li, Zhiping
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5638 - 5646
反应条件
tert.-butylhydroperoxide; iron(II) chloride in decane; acetonitrile
T=85°C; 1 h; Schlenk techniqueInert atmosphere;
参考文献
Li, Yuanming; Jia, Fan; Li, Zhiping
Chemistry - A European Journal, 2013 , vol. 19, # 1 p. 82 - 86
反应条件
copper diacetate; triethylamine in dichloromethane
40 h; Ambient temperature;
参考文献
Chan, Dominic M. T.
Tetrahedron Letters, 1996 , vol. 37, # 50 p. 9013 - 9016
反应条件
2,2'-azo-bisisobutyronitrile; potassium tert-butylate in benzene
T=110°C; 6 h;
参考文献
Bhakuni, Bhagat Singh; Kumar, Amit; Balkrishna, Shah Jaimin; Sheikh, Javeed Ahmed; Konar, Sanjit; Kumar, Sangit
Organic Letters, 2012 , vol. 14, # 11 p. 2838 - 2841
反应条件
tert.-butylhydroperoxide; iron(II) chloride in decane; acetonitrile
T=85°C; 1 h; Schlenk techniqueInert atmosphere; chemoselective reaction;
参考文献
Li, Yuanming; Jia, Fan; Li, Zhiping
Chemistry - A European Journal, 2013 , vol. 19, # 1 p. 82 - 86
反应条件
dysprosium
T=20°C; Inert atmosphere;
参考文献
Chen, Weifeng; Li, Kebin; Hu, Ziqiang; Wang, Liliang; Lai, Guoqiao; Li, Zhifang
Organometallics, 2011 , vol. 30, # 7 p. 2026 - 2030