N-甲基-N-苯基苯甲酰胺合成路线 （共 96 条）
反应条件
palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; trichlorophosphate
T=135°C; 6 h; Inert atmosphere;
参考文献
Sawant, Dinesh N.; Wagh, Yogesh S.; Bhatte, Kushal D.; Bhanage, Bhalchandra M.
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5489 - 5494
反应条件
tert.-butylhydroperoxide; iron(II) chloride in decane; acetonitrile
T=85°C; 1 h; Schlenk techniqueInert atmosphere; chemoselective reaction;
参考文献
Li, Yuanming; Jia, Fan; Li, Zhiping
Chemistry - A European Journal, 2013 , vol. 19, # 1 p. 82 - 86
反应条件
tert.-butylhydroperoxide; iron(II) chloride in decane; acetonitrile
T=85°C; 1 h; Schlenk techniqueInert atmosphere; chemoselective reaction;
参考文献
Li, Yuanming; Jia, Fan; Li, Zhiping
Chemistry - A European Journal, 2013 , vol. 19, # 1 p. 82 - 86
反应条件
triphenylphosphine
T=18 - 20°C;
参考文献
Parfenov, E. A.; Fomin, V. A.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 5 p. 1129 - 1137,947 - 953
反应条件
tert.-butylhydroperoxide; iron(II) chloride in decane; acetonitrile
T=85°C; 1 h; Schlenk techniqueInert atmosphere; chemoselective reaction;
参考文献
Li, Yuanming; Jia, Fan; Li, Zhiping
Chemistry - A European Journal, 2013 , vol. 19, # 1 p. 82 - 86
反应条件
1: pyridine / CH2Cl2
2: NaH / tetrahydrofuran / 20 °C
View Scheme
参考文献
Yamasaki, Ryu; Tanatani, Aya; Azumaya, Isao; Saito, Shoichi; Yamaguchi, Kentaro; Kagechika, Hiroyuki
Organic Letters, 2003 , vol. 5, # 8 p. 1265 - 1267
反应条件
2,2'-azo-bisisobutyronitrile; diphenyl diselenide; tri-n-butyl-tin hydride in benzene
1 h; Heatingother reagent: Bu3SnH/azobis(isobutyronitrile);
参考文献
Crich, David; Hwang, Jae-Taeg
Journal of Organic Chemistry, 1998 , vol. 63, # 8 p. 2765 - 2770
反应条件
palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; trichlorophosphate
T=165°C; 24 h; Inert atmosphere;
参考文献
Sawant, Dinesh N.; Wagh, Yogesh S.; Bhatte, Kushal D.; Bhanage, Bhalchandra M.
Journal of Organic Chemistry, 2011 , vol. 76, # 13 p. 5489 - 5494
反应条件
in diethyl ether
4 h; Ambient temperature;
参考文献
Okuwaki, Yukari; Inagawa, Yukiko; Tamamura, Hideo; Suzuki, Taeko; Kuwana, Hiroko; et al.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 187 - 190
反应条件
in tetrahydrofuran
Arylation;
参考文献
Katritzky, Alan R.; Monteux, Daphne A.; Tymoshenko, Dmytro O.; Belyakov, Sergei A.
Journal of Chemical Research - Part S, 1999 , # 3 p. 230 - 231
