N-甲基-N-苯基苯甲酰胺合成路线 （共 96 条）
反应条件
1: CH2Cl2 / 0.5 h / 0 °C
2: 1.) methyllithium / 1.) THF, 0 deg C, 1 h; 2.) THF, RT, overnight
View Scheme
参考文献
Tokitoh, Norihiro; Okazaki, Renji
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3291 - 3298
反应条件
oxygen in acetonitrile
electroreduction, Hg electrode;
参考文献
Voss, Juergen; Wiegand, Gabriele; Huelsmeyer, Karin
Chemische Berichte, 1985 , vol. 118, # 12 p. 4806 - 4820
反应条件
lithium hydride in benzene
96 h; Heating;
参考文献
Barton, Derek H. R.; Finet, Jean-Pierre; Motherwell, William B.; Pichon, Clotilde
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry, 1987 , p. 251 - 259
参考文献
v.Braun; Weissbach
Chemische Berichte, 1930 , vol. 63, p. 489,492
反应条件
1: 99 percent / pyridine / CH2Cl2 / Ambient temperature; overnight
2: 91 percent / diethyl ether / 4 h / Ambient temperature
View Scheme
参考文献
Okuwaki, Yukari; Inagawa, Yukiko; Tamamura, Hideo; Suzuki, Taeko; Kuwana, Hiroko; et al.
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 187 - 190
反应条件
1: 49 percent / Et3N / diethyl ether / 2 h / 20 °C
2: 1.) t-BuOK / 1.) THF, reflux, 2 h, 2.) 30 min
View Scheme
参考文献
Aitken, R. Alan; Raut, Swati V.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 7 p. 747 - 751
反应条件
1: 42 percent / triethylamine / benzene / 3 h / 0 °C
2: 42 percent / acetonitrile / 20 h / 80 °C
3: 52 percent / acetonitrile / 3 h / Ambient temperature
4: CDCl3 / 70 °C
View Scheme
参考文献
Symes, Jillian; Modro, Tomasz A.
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 39, p. 113 - 118
反应条件
1: triethylamine / dimethylformamide / 0.5 h / -20 °C
2: dimethylformamide / 20 h / -20 deg C to RT
View Scheme
参考文献
Shimagaki, Masayuki; Koshiji, Hiroko; Oishi, Takeshi
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 45 - 58
反应条件
1: APTS / xylene / 1 h / Heating
2: NaH / xylene; dimethylformamide
3: LiClO4, lutidine-2,6 / acetonitrile / electrooxydation; platine (S=16 cm2) comme anode; grafite (Φ=1 cm) comme cathode; 50 mA; +0.575 V/ECS; 1.75 F.mol-1
View Scheme
参考文献
Cariou, Michel; Carlier, Roger; Simonet, Jacques
Bulletin de la Societe Chimique de France, 1986 , # 5 p. 781 - 792
反应条件
1: 76 percent / triethylamine / diethyl ether
2: 94.5 percent / triphenylphosphine / 18 - 20 °C
View Scheme
参考文献
Parfenov, E. A.; Fomin, V. A.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 5 p. 1129 - 1137,947 - 953
