N-甲基-N-苯基苯甲酰胺合成路线 （共 96 条）
反应条件
1: cis-[Ru(CH3CN)2(η3-C3H5)(cod)]BF4; hydrogen; potassium hexamethylsilazane; 2-(diphenylphosphino)ethylamine / tetrahydrofuran / 24 h / 100 °C / 38002.6 Torr / Autoclave
2: triethylamine / dichloromethane / 0 - 20 °C / Inert atmosphere
View Scheme
参考文献
John, Jeremy M.; Bergens, Steven H.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 44 p. 10377 - 10380
反应条件
sodium hydride; xylene
und anschliessend mit Methyljodid;
参考文献
Jones
Journal of Organic Chemistry, 1949 , vol. 14, p. 1099,1101 Anm.1,1102
反应条件
methyllithium
1) THF, 0 deg C, 2) THF, r.t.; Yield given. Multistep reaction;
参考文献
Okazaki, Renji; Tokitoh, Norihiro
Journal of the Chemical Society, Chemical Communications, 1984 , # 3 p. 192 - 193
反应条件
in acetonitrile
60 h; Heating;
参考文献
Symes, Jillian; Modro, Tomasz A.
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 39, p. 113 - 118
反应条件
1: 42 percent / acetonitrile / 20 h / 80 °C
2: 52 percent / acetonitrile / 3 h / Ambient temperature
3: CDCl3 / 70 °C
View Scheme
参考文献
Symes, Jillian; Modro, Tomasz A.
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 39, p. 113 - 118
反应条件
in N,N-dimethyl-formamide
20 h; -20 deg C to RT; Yield given;
参考文献
Shimagaki, Masayuki; Koshiji, Hiroko; Oishi, Takeshi
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 45 - 58
反应条件
potassium tert-butylate
1.) THF, reflux, 2 h, 2.) 30 min; Yield given. Multistep reaction;
参考文献
Aitken, R. Alan; Raut, Swati V.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 7 p. 747 - 751
反应条件
silver(l) oxide; benzene
参考文献
Lander
Journal of the Chemical Society, 1902 , vol. 81, p. 595
Journal of the Chemical Society, 1903 , vol. 83, p. 412
反应条件
in acetonitrile
electroreduction, Hg electrode;
参考文献
Voss, Juergen; Wiegand, Gabriele; Huelsmeyer, Karin
Chemische Berichte, 1985 , vol. 118, # 12 p. 4806 - 4820
反应条件
in acetonitrile
electroreduction, Hg electrode;
参考文献
Voss, Juergen; Wiegand, Gabriele; Huelsmeyer, Karin
Chemische Berichte, 1985 , vol. 118, # 12 p. 4806 - 4820
