1,2,3,4-四氢-4-甲基喹啉合成路线 （共 24 条）
反应条件
hydrogen; phosphine free diamino rhodium catalyst in toluene T=120°C; P=51716.2 Torr; 48 h;
参考文献
Vasylyev, Maksym; Alper, Howard
Synthesis, 2010 , # 17 art. no. C03310SS, p. 2893 - 2900
反应条件
C26H29ClIrNO3; hydrogen in 2,2,2-trifluoroethanol T=40°C; P=760.051 Torr; 20 h;
参考文献
Wu, Jianjun; Barnard, Jonathan H.; Zhang, Yi; Talwar, Dinesh; Robertson, Craig M.; Xiao, Jianliang
Chemical Communications, 2013 , vol. 49, # 63 p. 7052 - 7054
反应条件
hydrogen; aluminum oxide; silica gel; nickel in various solvent(s) T=160°C; P=38786.1 Torr; 1.5 h;
参考文献
Journal of Heterocyclic Chemistry, , vol. 24, p. 1477 - 1483
反应条件
hydrogen; phosphine free diamino rhodium catalyst in toluene T=120°C; P=51716.2 Torr; 48 h;
参考文献
Chemical Communications, , # 26 p. 2710 - 2711
反应条件
trifluoroacetic acid
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 9, # 9 p. 1335 - 1340
反应条件
palladium 10 on activated carbon; zinc T=150°C; 24 h; Autoclave;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 9 p. 1826 - 1833
反应条件
1: DMAP / tetrahydrofuran 2: tetrahydrofuran / 0 °C 3: H2, TFA / Pd/C / ethyl acetate; ethanol 4: TFA View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 9, # 9 p. 1335 - 1340
反应条件
1: polyphosphoric acid / 100 °C 2: DMAP / tetrahydrofuran 3: tetrahydrofuran / 0 °C 4: H2, TFA / Pd/C / ethyl acetate; ethanol 5: TFA View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 9, # 9 p. 1335 - 1340
反应条件
1: toluene / 100 °C 2: polyphosphoric acid / 100 °C 3: DMAP / tetrahydrofuran 4: tetrahydrofuran / 0 °C 5: H2, TFA / Pd/C / ethyl acetate; ethanol 6: TFA View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 9, # 9 p. 1335 - 1340
反应条件
1: tetrahydrofuran / 0 °C 2: H2, TFA / Pd/C / ethyl acetate; ethanol 3: TFA View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 9, # 9 p. 1335 - 1340
