1,2,3,4-四氢-4-甲基喹啉合成路线 （共 24 条）
反应条件
bei der elektrochemischen Reduktion an einer Quecksilber-Kathode;
参考文献
Zhurnal Obshchei Khimii, , vol. 22, p. 2071,2074;engl.Ausg.S.2125,2126
反应条件
C21H21ClIrNO2 in tetrahydrofuran; 2,2,2-trifluoroethanol 20 h; Inert atmosphere;
参考文献
Wu, Jianjun; Talwar, Dinesh; Johnston, Steven; Yan, Ming; Xiao, Jianliang
Angewandte Chemie - International Edition, 2013 , vol. 52, # 27 p. 6983 - 6987
Ross. Khim. Zh., 2013 , vol. 125, # 27 p. 7121 - 7125,5
反应条件
1: conc. HCl, glacial HOAc / Heating
2: 55 percent / 20percent Pd-C / various solvent(s) / 21 h / 150 °C
View Scheme
参考文献
Rauckman; Tidwell; Johnson; Roth
Journal of Medicinal Chemistry, 1989 , vol. 32, # 8 p. 1927 - 1935
反应条件
1: conc. HCl, glacial HOAc / Heating
2: 55 percent / 20percent Pd-C / various solvent(s) / 21 h / 150 °C
3: 53 percent / conc. H2SO4, HNO3 / 1) 0 to 5 deg C, 30 min, 2) 25 deg C, 1 h
View Scheme
参考文献
Rauckman; Tidwell; Johnson; Roth
Journal of Medicinal Chemistry, 1989 , vol. 32, # 8 p. 1927 - 1935
