4-溴-1-(叔丁基二甲基硅基)吲哚合成路线 （共 2 条）
反应条件
1: 4-bromo-1H-indole With sodium hydride in tetrahydrofuran 1 h; 2: tert-butyldimethylsilyl chloride in tetrahydrofuran 2 h;
参考文献
Rafferty, Ryan J.; Williams, Robert M.
Journal of Organic Chemistry, 2012 , vol. 77, # 1 p. 519 - 524
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 1.5 h / -78 °C / |Inert atmosphere 1.2: -78 - 20 °C / |Inert atmosphere 2.1: sodium hydroxide / tetrahydrofuran; water / 20 °C / |Inert atmosphere View Scheme
参考文献
Xu, Xiao-Bo; Liu, Jian; Zhang, Jian-Jian; Wang, Ya-Wen; Peng, Yu
Organic Letters, 2013 , vol. 15, # 3 p. 550 - 553
