三甲基-[(E)-2-苯乙烯基]硅烷合成路线 （共 34 条）
反应条件
aluminium trichloride in dichloromethane 1.) -77 deg C, 45 min; 2.) from -77 deg C to r.t.;
参考文献
Bulletin de la Societe Chimique de France, , vol. 132, p. 559 - 568
反应条件
bis(dibenzylideneacetone)-palladium(0) in acetonitrile T=25°C; Yield given. Yields of byproduct given;
参考文献
Kikukawa, Kiyoshi; Ikenaga, Kazutoshi; Wada, Fumio; Matsuda, Tsutomu
Chemistry Letters, 1983 , p. 1337 - 1340
反应条件
aluminium trichloride in dichloromethane T=0°C; 0.5 h;
参考文献
Fleming, Ian; Pearce, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2485 - 2489
反应条件
tetracarbonylbis(μ-chloro)dirhodium(I) in 1,4-dioxane T=90°C; Narasaka acylation; 24 h;
参考文献
European Journal of Organic Chemistry, , # 19 p. 3219 - 3227
反应条件
1: 87 percent / CH2Cl2 / 4 h / 20 °C 2: 60 percent / KH / tetrahydrofuran; dimethylsulfoxide / 2 h / -30 °C View Scheme
参考文献
Watanabe; Kusumoto; Yoshida; Kataoka
Chemical Communications, 2001 , # 9 p. 839 - 840
反应条件
lithium chloride; copper dichloride; palladium dichloride in water T=20°C; 24 h; chemoselective reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 732, p. 15 - 20
反应条件
bis(η3-allyl-μ-chloropalladium(II)); TASF-(Et); triethyl phosphite in tetrahydrofuran T=50°C;
参考文献
Hatanaka, Yasuo; Hiyama, Tamejiro
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 918 - 920
反应条件
lithium chloride; copper dichloride; palladium dichloride in water T=20°C; 24 h; chemoselective reaction;
参考文献
Journal of Organometallic Chemistry, , vol. 732, p. 15 - 20
反应条件
bis(η3-allyl-μ-chloropalladium(II)); TASF-(Et); triethyl phosphite in tetrahydrofuran T=50°C;
参考文献
Hatanaka, Yasuo; Hiyama, Tamejiro
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 918 - 920
反应条件
sodium hydroxide; iodosylbenzene; boron trifluoride diethyl etherate 1.) CH2Cl2, r.t., 3 h, 2.) r.t.; Yield given. Multistep reaction;
参考文献
Ochiai, Masahito; Sumi, Kenzo; Nagao, Yoshimitsu; Fujita, Eiichi; Arimoto, Masao; Yamaguchi, Hideo
Journal of the Chemical Society, Chemical Communications, 1985 , # 11 p. 697 - 699
