反应条件
1: tin(IV) chloride / dichloromethane / -94 °C 2: trimethylsilyl bromide; triethylamine / acetonitrile / 18 h / -25 °C / |Inert atmosphere 3: silver nitrate / acetone; water / 3 h / |Reflux 4: acetic acid; zinc / 24 h 5: sodium cyanoborohydride / 1 h 6: hydrogen / methanol / 3.5 h / 20 °C / 18751.9 Torr / |Autoclave 7: dichloromethane / 2 h / 20 °C View Scheme
参考文献
Zhmurov, Petr A.; Sukhorukov, Alexey Yu.; Chupakhin, Vladimir I.; Khomutova, Yulia V.; Ioffe, Sema L.; Tartakovsky, Vladimir A.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 46 p. 8082 - 8091
