2-苯基-2,3-二氢-1H-异吲哚合成路线 (共 25 条)
反应条件
tert.-butylhydroperoxide; copper(l) chloride in dichloromethane; water T=50°C; 24 h; Sealed tube;
参考文献
Yan, Xiaoyu; Fang, Kun; Liu, Hailan; Xi, Chanjuan
Chemical Communications, 2013 , vol. 49, # 90 p. 10650 - 10652
反应条件
air in benzene T=20°C; 48 h;
参考文献
Doepp, Dietrich; Hassan, Alaa A.; Mourad, Aboul-Fetouh E.; Nour El-Din, Ahmed M.; Angermund, Klaus; Krueger, Carl; Lehmann, Christian W.; Rust, Joerg
Tetrahedron, 2003 , vol. 59, # 27 p. 5073 - 5081
反应条件
air; TNF in pyridine 5 h; Heating;
参考文献
Hassan, Alaa A.; Doepp, Dietrich; Henkel, Gerald
Journal of Heterocyclic Chemistry, 1998 , vol. 35, # 1 p. 121 - 128
反应条件
air 48 h; Ambient temperature;
参考文献
Hassan, Alaa A.
Journal of Chemical Research, Synopses, 1995 , # 12 p. 498 - 499
反应条件
sodium hydroxide in 1,4-dioxane
T=20°C; 0.2 h;
参考文献
Subbarayappa, Adimurthy; Patoliya, Paresh U.
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2009 , vol. 48, # 4 p. 545 - 552
反应条件
potassium carbonate in water
T=120°C; 0.333333 h; microwave irradiation;
参考文献
Ju, Yuhong; Varma, Rajender S.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 135 - 141
反应条件
potassium carbonate in water
T=105°C; 0.333333 h; Microwave irradiationGreen chemistry; Concentration;
参考文献
Barnard, T. Michael; Vanier, Grace S.; Collins Jr., Michael J.
Organic Process Research and Development, 2006 , vol. 10, # 6 p. 1233 - 1237
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; di-n-butylchlorotin hydride in tetrahydrofuran
T=0°C; Reduction; Amination; 1.5 h;
参考文献
Suwa, Toshihiro; Sugiyama, Erika; Shibata, Ikuya; Baba, Akio
Synthesis, 2000 , # 6 p. 789 - 800
反应条件
1: Lawesson reagent / toluene / Heating
2: 91 percent / benzene / Ambient temperature; Irradiation
3: 43 percent / Raney-Ni / methanol / 1 h / Ambient temperature
View Scheme
参考文献
Nishio, Takehiko; Okuda, Norikazu
Journal of Organic Chemistry, 1992 , vol. 57, # 14 p. 4000 - 4005
反应条件
1: 91 percent / benzene / Ambient temperature; Irradiation
2: 43 percent / Raney-Ni / methanol / 1 h / Ambient temperature
View Scheme
参考文献
Nishio, Takehiko; Okuda, Norikazu
Journal of Organic Chemistry, 1992 , vol. 57, # 14 p. 4000 - 4005