alpha-羟基呋喃-2-乙酸合成路线 (共 6 条)
反应条件
cesium fluoride in N,N-dimethyl-formamide T=60°C; P=760.051 Torr; 24 h;
参考文献
Mita, Tsuyoshi; Higuchi, Yuki; Sato, Yoshihiro
Organic Letters, 2014 , vol. 16, # 1 p. 14 - 17
反应条件
Al-Sn-beta in methanol; water T=84.84°C; 0.5 h; Reagent/catalyst;
参考文献
Schwartz, Thomas J.; Goodman, Samuel M.; Osmundsen, Christian M.; Taarning, Esben; Mozuch, Michael D.; Gaskell, Jill; Cullen, Daniel; Kersten, Philip J.; Dumesic, James A.
ACS Catalysis, 2013 , vol. 3, # 12 p. 2689 - 2693
反应条件
Sn-beta zeolites in tetrahydrofuran T=84.84°C; 3 h; Reagent/catalystTimeSolvent;
参考文献
Schwartz, Thomas J.; Goodman, Samuel M.; Osmundsen, Christian M.; Taarning, Esben; Mozuch, Michael D.; Gaskell, Jill; Cullen, Daniel; Kersten, Philip J.; Dumesic, James A.
ACS Catalysis, 2013 , vol. 3, # 12 p. 2689 - 2693
反应条件
Al-Sn-beta in methanol; water T=84.84°C; 0.5 h;
参考文献
Schwartz, Thomas J.; Goodman, Samuel M.; Osmundsen, Christian M.; Taarning, Esben; Mozuch, Michael D.; Gaskell, Jill; Cullen, Daniel; Kersten, Philip J.; Dumesic, James A.
ACS Catalysis, 2013 , vol. 3, # 12 p. 2689 - 2693
反应条件
1.1: lithium / tetrahydrofuran / 12 h / 0 °C / |Inert atmosphere 1.2: -78 °C / |Inert atmosphere 2.1: 3-keto-2H,3H-1,2-benzisothiazole 1,1-dioxide / dichloromethane / |Reflux; |Inert atmosphere 3.1: cesium fluoride / N,N-dimethyl-formamide / 24 h / 60 °C / 760.05 Torr View Scheme
参考文献
Mita, Tsuyoshi; Higuchi, Yuki; Sato, Yoshihiro
Organic Letters, 2014 , vol. 16, # 1 p. 14 - 17
反应条件
sodium tetrahydroborate in ethanol
参考文献
Chen, Yen Ting; Onaran; Doss, Christopher J.; Seto, Christopher T.
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 14 p. 1935 - 1938