N-(3-三氟甲基-苯基)-苯甲酰胺合成路线 (共 11 条)
反应条件
palladium diacetate; triethylamine in water T=100°C; P=5171.62 Torr; 8 h; Autoclave;
参考文献
Tambade, Pawan J.; Patil, Yogesh P.; Bhanushali, Mayur J.; Bhanage, Bhalchandra M.
Synthesis, 2008 , # 15 art. no. P04608SS, p. 2347 - 2352
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane T=20°C; Inert atmosphere;
参考文献
Panini, Piyush; Chopra, Deepak
CrystEngComm, 2012 , vol. 14, # 6 p. 1972 - 1989
反应条件
tris(dibenzylideneacetone)dipalladium (0); 1,3,4,6,7,8-hexahydro-1-methyl-2H-pyrimido{1,2-a}pyrimidine; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene T=150°C; 0.5 h; microwave irradiation;
参考文献
Tundel, Rachel E.; Anderson, Kevin W.; Buchwald, Stephen L.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 430 - 433
反应条件
copper(l) iodide; manganese(II) fluoride; rel-(R,R)-DACH; potassium hydroxide in water T=60°C; 24 h;
参考文献
Teo, Yong-Chua; Yong, Fui-Fong; Ithnin, Idzham Khalid; Yio, Siew-Hui Trionna; Lin, Zhiyin
European Journal of Organic Chemistry, 2013 , # 3 p. 515 - 524
反应条件
water in acetonitrile T=20°C; Flash photolysis;
参考文献
Ruane, Patrick H.; Ahmed, Abid R.; McClelland, Robert A.
Journal of the Chemical Society Perkin Transactions 2, 2002 , vol. 2, p. 312 - 317
反应条件
1: liquid ammonia; sodium amide View Scheme
参考文献
Benkeser; Severson
Journal of the American Chemical Society, 1949 , vol. 71, p. 3838
反应条件
1: 41 percent / DMAP; i-Pr2NEt / CH2Cl2 / 0 - 20 °C 2: 98 percent / 7-methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene; XantPhos; Pd2(dba)3 / toluene / 0.5 h / 150 °C / microwave irradiation View Scheme
参考文献
Tundel, Rachel E.; Anderson, Kevin W.; Buchwald, Stephen L.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 430 - 433
参考文献
Benkeser; Severson
Journal of the American Chemical Society, 1949 , vol. 71, p. 3838
反应条件
1: sodium hydride / tetrahydrofuran / Heating 2: water / acetonitrile / 20 °C / Flash photolysis View Scheme
参考文献
Ruane, Patrick H.; Ahmed, Abid R.; McClelland, Robert A.
Journal of the Chemical Society Perkin Transactions 2, 2002 , vol. 2, p. 312 - 317
反应条件
sodium hydroxide; sodium perchlorate in 1,4-dioxane; water T=25°C; various conc. of NaOH; Rate constantMechanism;
参考文献
Prudchenko, A. P.; Drizhd, L. P.; Savelova, V. A.
Journal of Organic Chemistry USSR (English Translation), 1986 , p. 923 - 926
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 5 p. 1029 - 1033