Fmoc-L-beta-高苯丙氨酸合成路线 (共 7 条)
反应条件
water; silver trifluoromethanesulfonate in 1,4-dioxane 72 h; sonication;
参考文献
Glenn, Matthew P.; Kelso, Michael J.; Tyndall, Joel D. A.; Fairlie, David P.
Journal of the American Chemical Society, 2003 , vol. 125, # 3 p. 640 - 641
反应条件
1: 94 percent / 1H-benzotriazol-1-yl-N-oxytrispyrrolidinophosphonium PF6(1-); N-ethyldiisopropylamine / tetrahydrofuran; dimethylformamide; diethyl ether / 0.25 h / 0 °C 2: 85 percent / silver benzoate / dioxane; H2O / 70 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 42, # 7 p. 1691 - 1695
反应条件
sodium carbonate in acetone pH=9 - 10; 6 h;
参考文献
Schreiber, Juerg V.; Seebach, Dieter
Helvetica Chimica Acta, 2000 , vol. 83, # 12 p. 3139 - 3152
反应条件
1: 92 percent / CH2Cl2 / 1 h / Ambient temperature 2: 50 percent / silver benzoate / dioxane; H2O / 70 °C View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 13 p. 1969 - 1971
反应条件
dimethyl sulfoxide T=120°C; 0.25 h; Microwave irradiation;
参考文献
Hoeck, Stefan; Marti, Roger; Riedl, Rainer; Simeunovic, Marina
Chimia, 2010 , vol. 64, # 3 p. 200 - 202
反应条件
dimethyl sulfoxide
T=120°C; 0.25 h; Microwave irradiation;
参考文献
Hoeck, Stefan; Marti, Roger; Riedl, Rainer; Simeunovic, Marina
Chimia, 2010 , vol. 64, # 3 p. 200 - 202
反应条件
dimethyl sulfoxide
T=120°C; 0.25 h; Microwave irradiation;
参考文献
Hoeck, Stefan; Marti, Roger; Riedl, Rainer; Simeunovic, Marina
Chimia, 2010 , vol. 64, # 3 p. 200 - 202