1: thien-2-yl bromide With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 2 h; 2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran; hexane T=-78 - 20°C; 3: With methanol in tetrahydrofuran; hexane
1: thiophene With n-butyllithium in tetrahydrofuran T=20°C; 0.5 h; 2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran T=20°C; 0.333333 h; Further stages.;
参考文献
Dienes, Yvonne; Durben, Stefan; Karpati, Tamas; Neumann, Toni; Englert, Ulli; Nyulaszi, Laszlo; Baumgartner, Thomas
Chemistry - A European Journal, 2007 , vol. 13, # 26 p. 7487 - 7500