4-溴-2,5-二氯苯甲胺合成路线 （共 8 条）
反应条件
hydrogenchloride; iron
参考文献
Sturala, Jiri; Cibulka, Radek
European Journal of Organic Chemistry, 2012 , # 36 p. 7066 - 7074
反应条件
1.1: hydrogen bromide; sodium nitrite / water / 0.08 h / -5 - 0 °C 1.2: 0.75 h / 20 - 50 °C 2.1: nitric acid / 2 h / 50 °C 3.1: FeCl3·6H2O; carbon; NH2NH2•xH2O / methanol / 4 h / |Reflux View Scheme
参考文献
Sturala, Jiri; Cibulka, Radek
European Journal of Organic Chemistry, 2012 , # 36 p. 7066 - 7074
反应条件
1: nitric acid / 2 h / 50 °C 2: FeCl3·6H2O; carbon; NH2NH2•xH2O / methanol / 4 h / |Reflux View Scheme
参考文献
Sturala, Jiri; Cibulka, Radek
European Journal of Organic Chemistry, 2012 , # 36 p. 7066 - 7074
反应条件
N-bromosuccinmide T=10°C; Solid phase reaction; bromination; 0.00833333 h;
参考文献
Sarma, Jagarlapudi A.R.P.; Nagaraju, Akula
Journal of the Chemical Society. Perkin Transactions 2, 2000 , # 6 p. 1113 - 1118
反应条件
ethanol; sulfuric acid
参考文献
Hurtley
Journal of the Chemical Society, 1901 , vol. 79, p. 1303
反应条件
1: glacial acetic acid / durch Chlorierung 2: alcohol; H2SO4 View Scheme
参考文献
Hurtley
Journal of the Chemical Society, 1901 , vol. 79, p. 1303
参考文献
Hurtley
Journal of the Chemical Society, 1901 , vol. 79, p. 1303
反应条件
sulfuric acid Diazotization.Kochen mit Wasser;
参考文献
Fox; Turner
Journal of the Chemical Society, 1930 , p. 1853,1860
