2,3-二氢-1H-吡啶并[3,4-b][1,4]噁嗪合成路线 (共 2 条)
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran
T=0 - 20°C; 1.5 h; Inert atmosphere;
2: With sodium hydroxide in tetrahydrofuran; water
T=0 - 20°C;
参考文献
Ahn, Sung Oh; Park, Chan Hee; Im, Jun Hwan; Lee, Soon Ok; Lee, Kyoung June; Cho, Seong Wook; Ko, Kwang Seok; Han, Sun Young; Lee, Won Il
Patent: US2011/28467 A1, 2011 ;
Location in patent: Page/Page column 16 ;
US 20110028467 A1
反应条件
hydrogenchloride in tetrahydrofuran; methanol; water
参考文献
C.D. Searle and Co.
Patent: US5652363 A1, 1997 ;