4-氨基-2,6-二硝基甲苯合成路线 （共 58 条）
参考文献
Koerner; Contardi
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1916 , vol. <5> 25 II, p. 348
Gazzetta Chimica Italiana, 1917 , vol. 47 I, p. 238
反应条件
1: 78 percent / 96percent H2SO4, 90percent HNO3 / acetic acid / 9 h / 0 °C
2: 35 percent / 96percent aq. H2SO4 / 60 h / 0 °C
3: 82 percent / 96percent aq. H2SO4, 20percent oleum, 98percent aq. hydrogen peroxide / Ambient temperature
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参考文献
Atkins, Ronald L.; Hollins, Richard A.; Wilson, William S.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3261 - 3266
反应条件
1: 78 percent / 96percent H2SO4, 90percent HNO3 / acetic acid / 9 h / 0 °C
2: 35 percent / 96percent aq. H2SO4 / 60 h / 0 °C
3: 82 percent / 96percent aq. H2SO4, 20percent oleum, 98percent aq. hydrogen peroxide / Ambient temperature
4: 74 percent / 0.4 N ammonia in dioxane / tetrahydrofuran / 0.17 h / Ambient temperature
View Scheme
参考文献
Atkins, Ronald L.; Hollins, Richard A.; Wilson, William S.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3261 - 3266
反应条件
Myriophyllum aquaticum in water
T=20°C; Reduction; 768 h; Enzymatic reaction; Product distributionKinetics;
参考文献
Bhadra; Spanggord; Wayment; Hughes; Shanks
Environmental Science and Technology, 1999 , vol. 33, # 19 p. 3354 - 3361
反应条件
Diazotization.Behandlung der Diazoniumsalz-Loesung mit KI;
参考文献
Parkes; Farthing
Journal of the Chemical Society, 1948 , p. 1275,1277
反应条件
nitric acid in dichloromethane; sulfuric acid; methoxybenzene
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US4426539 A1, 1984 ;
反应条件
1: conc. H2SO4, 90percent HNO3 / 3 h / 25 °C
2: 75 percent / conc. H2SO4, anisole / 0.75 h / 0 - 5 °C
View Scheme
参考文献
Atkins, Ronald L.; Hollins, Richard A.; Wilson, William S.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3261 - 3266
反应条件
nitric acid in dichloromethane; sulfuric acid; methoxybenzene
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US4426539 A1, 1984 ;
反应条件
1: 100 percent / 96percent aq. H2SO4, 90percent aq. HNO3 / 16 h / 0 - 5 °C
2: anisole, 96percent aq. H2SO4 / 0.5 h / Ambient temperature
View Scheme
参考文献
Atkins, Ronald L.; Hollins, Richard A.; Wilson, William S.
Journal of Organic Chemistry, 1986 , vol. 51, # 17 p. 3261 - 3266
参考文献
Morgan; Clayton
Journal of the Chemical Society, 1910 , vol. 97, p. 2650
