4-氨基-2,6-二硝基甲苯合成路线 (共 58 条)
反应条件
nitronium tetrafluoroborate powder in water; 1,2-dichloro-ethane
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US4451681 A1, 1984 ;
反应条件
nitric acid in dichloromethane; acetic acid
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US4451681 A1, 1984 ;
反应条件
in 1,4-dioxane; (2S)-N-methyl-1-phenylpropan-2-amine hydrate
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US4248798 A1, 1981 ;
反应条件
ozone in water
Oxidation; pH=5.0; Product distribution;
参考文献
Spanggord, Ronald J.; Yao, C. David; Mill, Theodore
Environmental Science and Technology, 2000 , vol. 34, # 3 p. 497 - 504
反应条件
1: aqueous H2SO4 / <0 / Diazotization.Eintragen der Diazoniumsalz-Loesung in siedende wss. CuSO4-Loesung
2: aqueous KOH
3: aqueous HCl; tin / 70 - 80 °C / Kochen des Reaktionsprodukts mit Wasser unter Kohlendioxyd
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参考文献
Curd; Robertson
Journal of the Chemical Society, 1933 , p. 437,440
反应条件
sulfuric acid
Diazotization.Eintragen der Diazoniumsalz-Loesung in siedende wss. CuSO4-Loesung;
参考文献
Curd; Robertson
Journal of the Chemical Society, 1933 , p. 437,440
反应条件
2: H2S; alcohol; ammonia / Kochen des entstandenen 4-Chlor-6-nitro-2-hydroxylamino-toluols mit Salzsaeure + KI
3: Ersatz der NH2-Gruppe durch Chlor
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参考文献
Cohen; Mc Candlish
Journal of the Chemical Society, 1905 , vol. 87, p. 1265
反应条件
1: sodium acetate; glacial acetic acid; bromine
2: nitric acid; nitrogen oxides / 0 °C / Behandeln des entstandenen Diazoniumnitrats mit NaNO2
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参考文献
Koerner; Contardi
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1916 , vol. <5> 25 II, p. 348
Gazzetta Chimica Italiana, 1917 , vol. 47 I, p. 238