3,3,5,5-四甲基吗啉合成路线 （共 3 条）
反应条件
sodium hydroxide; methanesulfonic acid
参考文献
The B. F. Goodrich Company
Patent: US4914232 A1, 1990 ;
Title/Abstract Full Text Show Details
Lai; John T.
Patent: US4528370 A1, 1985 ;
反应条件
1: With lithium aluminium tetrahydride Inert atmosphere; 2: With methanesulfonic acid Inert atmosphere;
参考文献
Sumerin, Victor; Chernichenko, Konstantin; Nieger, Martin; Leskelae, Markku; Rieger, Bernhard; Repo, Timo
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2093 - 2110
反应条件
1: 1.) conc. aq. HCl, 2.) (C2H5)3N / 1.) reflux, 15 h, 2.) reflux, 6 h 2: 90 percent / LiAlH4 / tetrahydrofuran / 3 h / Heating 3: 43 percent / methanesulfonic acid / 18 h / 140 °C View Scheme
参考文献
Synthesis, , # 2 p. 122 - 123
