1-硝基-4-苯基乙炔苯合成路线 (共 107 条)
反应条件
polymer supported palladium catalyst in N,N-dimethyl-formamide
T=70°C; Stille coupling reaction; 0.17 h;
参考文献
Dell'Anna, Maria Michela; Lofu, Antonio; Mastrorilli, Piero; Mucciante, Vittoria; Nobile, Cosimo Francesco
Journal of Organometallic Chemistry, 2006 , vol. 691, # 1-2 p. 131 - 137
反应条件
polymer supported palladium catalyst in N,N-dimethyl-formamide
T=70°C; Stille coupling reaction; 13 h;
参考文献
Dell'Anna, Maria Michela; Lofu, Antonio; Mastrorilli, Piero; Mucciante, Vittoria; Nobile, Cosimo Francesco
Journal of Organometallic Chemistry, 2006 , vol. 691, # 1-2 p. 131 - 137
反应条件
1,4-diaza-bicyclo[2.2.2]octane; triphenylphosphine; tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran
T=20°C; P=760.051 Torr; 6 h;
参考文献
Iizuka, Muneaki; Kondo, Yoshinori
European Journal of Organic Chemistry, 2007 , # 31 p. 5180 - 5182
反应条件
tetrakis(triphenylphosphine) palladium(0); lithium chloride in tetrahydrofuran; N,N-dimethyl-formamide
T=80°C; 12 h;
参考文献
Chen, Qing-Yun; He, Ya-Bo
Tetrahedron Letters, 1987 , vol. 28, # 21 p. 2387 - 2388
反应条件
copper(l) iodide; cesium fluoride in toluene; acetonitrile
T=150°C; 0.5 h; Inert atmosphereMicrowave irradiation;
参考文献
Akubathini, Shashidhar Kumar; Biehl, Ed
Tetrahedron Letters, 2009 , vol. 50, # 16 p. 1809 - 1811
反应条件
palladium diacetate; triethylamine; triphenylphosphine in dimethyl sulfoxide
T=65°C; Sonogashira coupling; 16 h; Inert atmosphere;
参考文献
Shirbin, Steven J.; Boughton, Berin A.; Zammit, Steven C.; Zanatta, Shannon D.; Marcuccio, Sebastian M.; Hutton, Craig A.; Williams, Spencer J.
Tetrahedron Letters, 2010 , vol. 51, # 22 p. 2971 - 2974
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=90°C; 2 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Jadhav, Deepak N.; Dasgupta, Priyabrata
Organic Letters, 2010 , vol. 12, # 9 p. 2048 - 2051
反应条件
copper(l) iodide; [Pt(PPh3)4] in N,N-dimethyl-formamide
T=120°C; 12 h;
参考文献
Oh, Chang Ho; Reddy, V. Raghava
Synlett, 2004 , # 12 p. 2091 - 2094
反应条件
triethylamine; AgCl; palladium dichloride in acetonitrile
T=20°C; Sonogashira coupling; 0.666667 h;
参考文献
Zhu, Min; Zhou, Zhongshi; Chen, Rui
Synthesis, 2008 , # 17 art. no. P04108SS, p. 2680 - 2682
反应条件
copper(l) iodide; triethylamine in N,N-dimethyl-formamide
T=90°C; Sonogashira coupling; 10 h;
参考文献
Bhunia, Susmita; Koner, Subratanath
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 2011 , vol. 50, # 9-10 p. 1380 - 1387