1-叔丁基-4,4-二氟环己烷合成路线 （共 21 条）
反应条件
Sm(HMDS)2 in hexane T=100°C; 1 h; Microwave irradiationInert atmosphereGlovebox;
参考文献
Janjetovic, Mario; Traeff, Annika M.; Ankner, Tobias; Wettergren, Jenny; Hilmersson, Goeran
Chemical Communications, 2013 , vol. 49, # 18 p. 1826 - 1828
反应条件
ethanol; [bis(2-methoxyethyl)amino]-sulfur trifluoride in dichloromethane
16 h; Ambient temperature;
参考文献
Beaulieu, Francis; Beauregard, Louis-Philippe; Courchesne, Gabriel; Couturier, Michel; Laflamme, Francois; L'Heureux, Alexandre
Organic Letters, 2009 , vol. 11, # 21 p. 5050 - 5053
反应条件
BF3.OEt2 in dichloromethane
参考文献
Air Products and Chemicals, Inc.
Patent: US6222064 B1, 2001 ;
反应条件
BF3.OEt2 in dichloromethane
参考文献
Air Products and Chemicals, Inc.
Patent: US6222064 B1, 2001 ;
反应条件
BF3.OEt2; Diethylaminosulfur trifluoride in dichloromethane
参考文献
Air Products and Chemicals, Inc.
Patent: US6222064 B1, 2001 ;
反应条件
iodine monofluoride in chloroform
1 h; Ambient temperature;
参考文献
Rozen, Shlomo; Zamir, Dov
Journal of Organic Chemistry, 1991 , vol. 56, # 15 p. 4695 - 4700
反应条件
bromine trifluoride in monofluoro-trichloromethane
参考文献
Rozen, Shlomo; Mishani, Eyal; Bar-Haim, Arie
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 2918
反应条件
iodine monofluoride in monofluoro-trichloromethane
T=-78°C; Yield given. Yields of byproduct given;
参考文献
Rozen, Shlomo; Brand, Michael; Zamir, Dov; Hebel, David
Journal of the American Chemical Society, 1987 , vol. 109, # 3 p. 896 - 897
反应条件
bromine trifluoride in monofluoro-trichloromethane
参考文献
Rozen, Shlomo; Mishani, Eyal; Bar-Haim, Arie
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 2918
反应条件
in ethanol; dichloromethane
参考文献
Air Products and Chemicals, Inc.
Patent: US6080886 A1, 2000 ;
