1-叔丁基-4,4-二氟环己烷合成路线 (共 21 条)
反应条件
iodine monofluoride in chloroform
1 h; Ambient temperature;
参考文献
Rozen, Shlomo; Zamir, Dov
Journal of Organic Chemistry, 1991 , vol. 56, # 15 p. 4695 - 4700
反应条件
iodine monofluoride in chloroform
1 h; Ambient temperature;
参考文献
Rozen, Shlomo; Zamir, Dov
Journal of Organic Chemistry, 1991 , vol. 56, # 15 p. 4695 - 4700
反应条件
iodine monofluoride in chloroform
1 h; Ambient temperature;
参考文献
Rozen, Shlomo; Zamir, Dov
Journal of Organic Chemistry, 1991 , vol. 56, # 15 p. 4695 - 4700
反应条件
bromine trifluoride in monofluoro-trichloromethane
参考文献
Rozen, Shlomo; Mishani, Eyal; Bar-Haim, Arie
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 2918
反应条件
iodine monofluoride in chloroform
2 h; Ambient temperature;
参考文献
Rozen, Shlomo; Zamir, Dov
Journal of Organic Chemistry, 1991 , vol. 56, # 15 p. 4695 - 4700
反应条件
triethylamine tris(hydrogen fluoride); triethylamine; Xtalfluor-E® in dichloromethane
T=20°C; 24 h; Inert atmosphere;
参考文献
Lheureux, Alexandre; Beaulieu, Francis; Bennett, Christopher; Bill, David R.; Clayton, Simon; Laflamme, Franois; Mirmehrabi, Mahmoud; Tadayon, Sam; Tovell, David; Couturier, Michel
Journal of Organic Chemistry, 2010 , vol. 75, # 10 p. 3401 - 3411
参考文献
Eliel,E.L.; Martin,R.J.L.
Journal of the American Chemical Society, 1968 , vol. 90, p. 682 - 689
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
1 h; Ambient temperature; Yield given;
参考文献
Rozen, Shlomo; Zamir, Dov
Journal of Organic Chemistry, 1991 , vol. 56, # 15 p. 4695 - 4700
反应条件
lithium aluminium tetrahydride; iodine monofluoride
1) CHCl3, r.t., 1 h, 2) THF, r.t., 1 h; Yield given. Multistep reaction;
参考文献
Rozen, Shlomo; Zamir, Dov
Journal of Organic Chemistry, 1991 , vol. 56, # 15 p. 4695 - 4700
反应条件
lithium aluminium tetrahydride; iodine monofluoride
1) CHCl3, r.t., 1 h, 2) THF, r.t., 1 h; Yield given. Multistep reaction;
参考文献
Rozen, Shlomo; Zamir, Dov
Journal of Organic Chemistry, 1991 , vol. 56, # 15 p. 4695 - 4700