甲基(4-硝基苯基)氨基甲酸酯合成路线 （共 24 条）
反应条件
1,3-dibromo-5,5-dimethyl-hydantoin; mercury(II) diacetate in N,N-dimethyl-formamide T=45°C; 12 h;
参考文献
Jew, Sang-sup; Park, Hyeung Geun; Park, Hee-Joo; Park, Min-soo; Cho, Youn-sang
Tetrahedron Letters, 1990 , vol. 31, # 11 p. 1559 - 1562
反应条件
indium in acetonitrile T=20°C; 12 h; Inert atmosphere;
参考文献
Kim, Joong-Gon; Jang, Doo Ok
Tetrahedron Letters, 2009 , vol. 50, # 22 p. 2688 - 2692
反应条件
carbon monoxide; Pd(phen)2(OTf)2 in methanol; chlorobenzene T=135°C; P=45003.6 Torr; 2 h; Yield given. Yields of byproduct given;
参考文献
Wehman, Petra; Kamer, Paul C. J.; Van Leeuwen, Piet W. N. M.
Chemical Communications, 1996 , # 2 p. 217 - 218
反应条件
1: oxalyl dichloride; 4-nitro-aniline With hydrogenchloride in 1,4-dioxane; ethyl acetate T=5 - 10°C; 2: in 1,4-dioxane; 1,2-dichloro-benzene T=130°C; 2 h; 3: methanol in 1,4-dioxane; 1,2-dichloro-benzene T=20 - 30°C; Further stages.;
参考文献
Oh, Lynette M.; Spoors, P. Grant; Goodman, Richard M.
Tetrahedron Letters, 2004 , vol. 45, # 24 p. 4769 - 4771
参考文献
Garofalo, Antonio; Goossens, Laurence; Six, Perrine; Lebegue, Nicolas; Depreux, Patrick
Synthetic Communications, 2011 , vol. 41, # 13 p. 2007 - 2016
反应条件
18-crown-6 ether; sodium hydride T=50°C;
参考文献
Lissel, Manfred; Rohani-Dezfuli, Ali Reza; Vogt, Gabriele
Journal of Chemical Research, Miniprint, 1989 , # 10 p. 2434 - 2452
反应条件
Pd(phen)2(OTf)2; 2-chloro-5-carboxybenzene in chlorobenzene T=135°C; P=45003.6 Torr; 2 h; Yield given. Yields of byproduct given;
参考文献
Wehman, Petra; Kamer, Paul C. J.; Van Leeuwen, Piet W. N. M.
Chemical Communications, 1996 , # 2 p. 217 - 218
反应条件
nitric acid T=70 - 80°C; Oxidation; 1 h;
参考文献
Velikorodov
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 2 p. 233 - 239
反应条件
18-crown-6 ether; potassium carbonate T=90°C; 12 h;
参考文献
Lissel, Manfred; Rohani-Dezfuli, Ali Reza; Vogt, Gabriele
Journal of Chemical Research, Miniprint, 1989 , # 10 p. 2434 - 2452
反应条件
Pd(phen)2(OTf)2; 2-chloro-5-carboxybenzene in chlorobenzene T=135°C; P=45003.6 Torr; 5 h; other time; also without cocatalyst; also for further aromatic nitro compounds; Product distribution;
参考文献
Wehman, Petra; Kamer, Paul C. J.; Van Leeuwen, Piet W. N. M.
Chemical Communications, 1996 , # 2 p. 217 - 218
