甲基(4-硝基苯基)氨基甲酸酯合成路线 (共 24 条)
反应条件
1: tetraethylammonium bromide; potassium superoxide / dimethylformamide / 20 °C 2: dimethylformamide View Scheme
参考文献
Usharani; Bhujanga Rao; Reddy; Dubey
Asian Journal of Chemistry, 2011 , vol. 23, # 4 p. 1802 - 1806
反应条件
1: 65 percent / HSO3ONO / acetic acid / 0.5 h / 0 °C 2: 79 percent / aq. HNO3 / 1 h / 70 - 80 °C View Scheme
参考文献
Velikorodov
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 2 p. 233 - 239
反应条件
1: TolSO2N=IPh / dichloromethane / 1.5 h / 20 °C / Inert atmosphere 2: dichloromethane / 4.5 h / 20 °C / Inert atmosphere View Scheme
参考文献
Yoshimura, Akira; Luedtke, Matthew W.; Zhdankin, Viktor V.
Journal of Organic Chemistry, 2012 , vol. 77, # 4 p. 2087 - 2091
反应条件
1: carbon monoxide With potassium superoxide; tetrabutylammomium bromide in N,N-dimethyl-formamide 0.25 h; 2: 4-nitro-aniline in N,N-dimethyl-formamide 0.0833333 h; Microwave irradiation; 3: methyl iodide in N,N-dimethyl-formamide
参考文献
Singh, Satish Kumar; Verma, Manjusha; Singh, Krishna Nand
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2008 , vol. 47, # 10 p. 1545 - 1548
反应条件
in N,N-dimethyl-formamide
参考文献
Singh, Krishna Nand
Synthetic Communications, 2007 , vol. 37, # 16 p. 2651 - 2654
参考文献
Hutchby, Marc; Houlden, Chris E.; Gair Ford; Tyler, Simon N. G.; Gagne, Michel R.; Lloyd-Jones, Guy C.; Booker-Milburn, Kevin I.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 46 p. 8721 - 8724
反应条件
sulfuric acid T=50°C; 3 h; var. alkyl N-carbamates; Product distributionMechanism;
参考文献
Wilshire, John F. K.
Australian Journal of Chemistry, 1990 , vol. 43, # 11 p. 1817 - 1826
反应条件
KY zeolite T=150°C; 10 h; other zeolite reagent; different reaction time and temperature; Product distribution;
参考文献
Selva, Maurizio; Bomben, Andrea; Tundo, Pietro
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 7 p. 1041 - 1045
反应条件
T=20°C; Rate constant;
参考文献
Baker; Holdsworth
Journal of the Chemical Society, 1947 , p. 713,723
反应条件
in methanol; anhydrous xylene; water
参考文献
Reanal Finomvegyszergyar
Patent: US4410697 A1, 1983 ;