3-(N,N-二乙基)氨基-4-甲氧基乙酰苯胺合成路线 （共 5 条）
反应条件
potassium carbonate in dichloromethane
参考文献
Watanabe, Tetsushi; Shiozawa, Tatsushi; Takahashi, Yoshifumi; Takahashi, Tomoyuki; Terao, Yoshiyasu; Nukaya, Haruo; Takamura, Takeji; Sawanishi, Hiroyuki; Ohe, Takeshi; Hirayama, Teruhisa; Wakabayashi, Keiji
Mutagenesis, 2002 , vol. 17, # 4 p. 293 - 299
反应条件
1: 2,4-dinitro-6-bromo-aniline With sulfuric acid; sodium nitrite 2: 3-acetylamino-6-methoxy-N,N-diethylaniline Further stages.;
参考文献
Watanabe, Tetsushi; Shiozawa, Tatsushi; Takahashi, Yoshifumi; Takahashi, Tomoyuki; Terao, Yoshiyasu; Nukaya, Haruo; Takamura, Takeji; Sawanishi, Hiroyuki; Ohe, Takeshi; Hirayama, Teruhisa; Wakabayashi, Keiji
Mutagenesis, 2002 , vol. 17, # 4 p. 293 - 299
反应条件
1: nitrosyl-sulphuric acid; 2,4-dinitro-6-bromo-aniline in sulfuric acid T=20 - 25°C; 1 h; 2: 3-acetylamino-6-methoxy-N,N-diethylaniline in H2O; sulfamic acid; sulfuric acid T=0 - 5°C; pH=4 - 4.5; 2 h;
参考文献
DyStar Textilfarben GmbH and Co. Deutschland KG
Patent: EP1188799 A1, 2002 ;
Location in patent: Example 5 ;
