5-氨基-(1,1'-联苯)-2-醇合成路线 （共 8 条）
反应条件
hydrogen; palladium on activated charcoal in methanol P=2068.59 Torr; 2 h;
参考文献
Dickerson, Tobin J.; Tremblay, Martin R.; Hoffman, Timothy Z.; Ruiz, Diana I.; Janda, Kim D.
Journal of the American Chemical Society, 2003 , vol. 125, # 50 p. 15395 - 15401
反应条件
boron tribromide in dichloromethane T=0°C; 0.333333 h;
参考文献
Moran, Edmund J.; Jacobsen, John R.; Leadbetter, Michael R.; Nodwell, Matthew B.; Trapp, Sean G.; Aggen, James; Church, Timothy J.
Patent: US2003/229058 A1, 2003 ;
Location in patent: Page 41 ;
US 20030229058 A1
反应条件
hydrogen; 5 palladium over charcoal in methanol 3 h;
参考文献
SCHERING CORPORATION
Patent: WO2007/97937 A1, 2007 ;
Location in patent: Page/Page column 176 ;
WO 2007/097937 A1
反应条件
1: 19 percent / nitric acid / acetic acid / 2 h / 20 °C 2: 98 percent / H2 / Pd/C / methanol / 2 h / 2068.59 Torr View Scheme
参考文献
Werbel; Cook; Elslager; Hung; Johnson; Kesten; McNamara; Ortwine; Worth
Journal of Medicinal Chemistry, 1986 , vol. 29, # 6 p. 924 - 939
反应条件
sodium dithionite; sodium carbonate T=35°C; 5 h;
参考文献
Werbel; Cook; Elslager; Hung; Johnson; Kesten; McNamara; Ortwine; Worth
Journal of Medicinal Chemistry, 1986 , vol. 29, # 6 p. 924 - 939
反应条件
Behandeln des Reaktionsprodukts mit wss.Natriumdithionit;
参考文献
Pilski, J.; Court, J.; Eustathopoulos, H.; Bonnier, J. M.
Tetrahedron, 1985 , vol. 41, # 19 p. 4331 - 4338
反应条件
in ethanol 0.3 h; Ambient temperatureIrradiation;
参考文献
Haga, Naoki; Takayanagi, Hiroaki
Journal of Organic Chemistry, 1996 , vol. 61, # 2 p. 735 - 745
参考文献
Pilski, J.; Court, J.; Eustathopoulos, H.; Bonnier, J. M.
Tetrahedron, 1985 , vol. 41, # 19 p. 4331 - 4338
