N1,n4-二乙基丁烷-1,4-二胺合成路线 (共 8 条)
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether 2 h; Heating;
参考文献
Kuehne, Hardy; Hesse, Manfred
Helvetica Chimica Acta, 1982 , vol. 65, # 5 p. 1470 - 1481
反应条件
hydrogen; Lindlar's catalyst in propan-1-ol; ethanol
参考文献
Chekulaeva,I.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1967 , p. 1752 - 1754
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1967 , p. 1829 - 1832
反应条件
lithium aluminium tetrahydride
参考文献
Surrey,A.R.; Mayer,J.R.
Journal of Medicinal and Pharmaceutical Chemistry, 1961 , vol. 3, p. 419 - 425
反应条件
perchloric acid; sodium perchlorate; dihydrogen peroxide; iron(II) sulfate T=45°C; activation energy 153 KJ mol-1; determination of velocity constants in dependence on temperature, concentration of hydrogen peroxide, and substrate concentration; Rate constantKineticsThermodynamic data;
参考文献
Ahmad, Iftikhar; Rauf, A. M. A.; Saeed, Kamal M.
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 1 p. 23 - 28
反应条件
transamination, boiling under inert atmosphere, distn. of dimethylamine during the reaction; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
transamination, boiling under inert atmosphere, distn. of dimethylamine during the reaction; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
transamination, boiling under inert atmosphere, distn. of dimethylamine during the reaction; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
参考文献
Mitsui Toatsu Chemicals, Inc.
Patent: US4918186 A1, 1990 ;