2,3,4,5,6-五氟二苯基甲醛合成路线 （共 9 条）
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=-78 - 20°C; 2.5 h;
参考文献
Dilman; Arkhipov; Belyakov; Struchkova; Tartakovsky
Russian Chemical Bulletin, 2006 , vol. 55, # 3 p. 517 - 522
反应条件
in diethyl ether reaction at 0°C, 1 hour;;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 1.3.3.8, page 33 - 59
反应条件
hydrogenchloride; water in tetrahydrofuran; methanol T=20°C; 1 h; Inert atmosphere;
参考文献
Brogan, Samatha; Carter, Neil B.; Lam, Hon Wai
Synlett, 2010 , # 4 art. no. D30809ST, p. 615 - 617
反应条件
1: i-PrMgBr / tetrahydrofuran / 0.5 h / -78 °C View Scheme
参考文献
Abarbri, Mohamed; Dehmel, Florian; Knochel, Paul
Tetrahedron Letters, 1999 , vol. 40, # 42 p. 7449 - 7453
反应条件
Grignard reaction; alkylation;
参考文献
Gmelin Handbook: F: PerFHalOrg.4, 2.2.4, page 68 - 115
反应条件
hydrogenchloride; TASF-(Et) 1.) THF, room temperature, 12 h; 2.) room temperature, methanol; Yield given. Multistep reaction;
参考文献
Fujita, Makoto; Obayashi, Michio; Hiyama, Tamejiro
Tetrahedron, 1988 , vol. 44, # 13 p. 4135 - 4146
反应条件
(i) Mg, (ii) /BRN= 471223/; Multistep reaction;
参考文献
Barbour,A.K. et al.
Journal of the Chemical Society, 1961 , p. 808 - 817
反应条件
in methanol; dimethylsulfoxide-d6 Kinetics;
参考文献
Tetrahedron Letters, , vol. 47, # 42 p. 7405 - 7407
反应条件
chromium(VI) oxide; acetic acid
参考文献
Barbour,A.K. et al.
Journal of the Chemical Society, 1961 , p. 808 - 817
